ソフトウェア 名称 バージョン 分類 SBC-Collectデータ収集 MOLREP位相決定 REFMAC5.5.0109精密化 HKL-3000データ削減 HKL-3000データスケーリング
精密化 構造決定の手法 : 分子置換開始モデル : 1XC4解像度 : 2.1→40 Å / Cor.coef. Fo :Fc : 0.949 / Cor.coef. Fo :Fc free : 0.916 / SU B : 11.182 / SU ML : 0.134 / 交差検証法 : THROUGHOUT / σ(F) : 2 / σ(I) : 2 / ESU R Free : 0.196 / 立体化学のターゲット値 : MAXIMUM LIKELIHOOD / 詳細 : HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONSRfactor 反射数 %反射 Selection details Rfree 0.23304 1491 5.1 % RANDOM Rwork 0.17914 - - - obs 0.18201 27827 99.32 % - all - 29318 - -
溶媒の処理 イオンプローブ半径 : 0.8 Å / 減衰半径 : 0.8 Å / VDWプローブ半径 : 1.4 Å / 溶媒モデル : MASK原子変位パラメータ Biso mean : 23.31 Å2 Baniso -1 Baniso -2 Baniso -3 1- 0.91 Å2 0 Å2 0 Å2 2- - -1 Å2 0 Å2 3- - - 0.09 Å2
精密化ステップ サイクル : LAST / 解像度 : 2.1→40 Åタンパク質 核酸 リガンド 溶媒 全体 原子数 3882 0 4 381 4267
拘束条件 大きな表を表示 (5 x 33) 大きな表を隠す Refine-ID タイプ Dev ideal Dev ideal target 数 X-RAY DIFFRACTION r_bond_refined_d0.02 0.022 3965 X-RAY DIFFRACTION r_bond_other_d0.001 0.02 2634 X-RAY DIFFRACTION r_angle_refined_deg1.668 1.979 5396 X-RAY DIFFRACTION r_angle_other_deg1.17 3 6483 X-RAY DIFFRACTION r_dihedral_angle_1_deg6.231 5 517 X-RAY DIFFRACTION r_dihedral_angle_2_deg37.029 25.273 165 X-RAY DIFFRACTION r_dihedral_angle_3_deg14.876 15 632 X-RAY DIFFRACTION r_dihedral_angle_4_deg20.284 15 19 X-RAY DIFFRACTION r_chiral_restr0.097 0.2 628 X-RAY DIFFRACTION r_gen_planes_refined0.009 0.021 4456 X-RAY DIFFRACTION r_gen_planes_other0.001 0.02 731 X-RAY DIFFRACTION r_nbd_refinedX-RAY DIFFRACTION r_nbd_otherX-RAY DIFFRACTION r_nbtor_refinedX-RAY DIFFRACTION r_nbtor_otherX-RAY DIFFRACTION r_xyhbond_nbd_refinedX-RAY DIFFRACTION r_xyhbond_nbd_otherX-RAY DIFFRACTION r_metal_ion_refinedX-RAY DIFFRACTION r_metal_ion_otherX-RAY DIFFRACTION r_symmetry_vdw_refinedX-RAY DIFFRACTION r_symmetry_vdw_otherX-RAY DIFFRACTION r_symmetry_hbond_refinedX-RAY DIFFRACTION r_symmetry_hbond_otherX-RAY DIFFRACTION r_symmetry_metal_ion_refinedX-RAY DIFFRACTION r_symmetry_metal_ion_otherX-RAY DIFFRACTION r_mcbond_it1.03 1.5 2597 X-RAY DIFFRACTION r_mcbond_other0.201 1.5 1034 X-RAY DIFFRACTION r_mcangle_it1.889 2 4157 X-RAY DIFFRACTION r_scbond_it2.645 3 1368 X-RAY DIFFRACTION r_scangle_it4.429 4.5 1238 X-RAY DIFFRACTION r_rigid_bond_restrX-RAY DIFFRACTION r_sphericity_freeX-RAY DIFFRACTION r_sphericity_bonded
LS精密化 シェル 解像度 : 2.1→2.154 Å / Total num. of bins used : 20 Rfactor 反射数 %反射 Rfree 0.277 104 - Rwork 0.193 2028 - obs - - 99.58 %
精密化 TLS 手法 : refined / Refine-ID : X-RAY DIFFRACTION
大きな表を表示 (25 x 30) 大きな表を隠す ID L11 (°2 )L12 (°2 )L13 (°2 )L22 (°2 )L23 (°2 )L33 (°2 )S11 (Å °)S12 (Å °)S13 (Å °)S21 (Å °)S22 (Å °)S23 (Å °)S31 (Å °)S32 (Å °)S33 (Å °)T11 (Å2 )T12 (Å2 )T13 (Å2 )T22 (Å2 )T23 (Å2 )T33 (Å2 )Origin x (Å)Origin y (Å)Origin z (Å)1 5.2696 0.5861 3.5762 0.3159 -0.5421 2.2062 -0.0953 0.1292 0.3951 -0.0729 -0.0478 0.1078 -0.0506 0.2334 0.1431 0.4348 -0.0226 0.0623 0.1272 -0.0151 0.1986 15.7165 17.6073 18.5461 2 0.7552 -0.1566 0.3761 2.5201 -1.7015 1.5979 0.0385 -0.016 0.0292 -0.2394 0.0239 0.0975 -0.0165 -0.0994 -0.0624 0.2609 0.0055 -0.0043 0.2033 -0.0005 0.1972 8.1701 10.3718 14.2814 3 0.5274 0.1307 0.3464 1.0091 -0.2778 1.0616 -0.0105 0.0694 0.007 -0.0204 -0.032 -0.0933 0.0854 0.1017 0.0425 0.2096 0.0085 0.0016 0.2115 -0.0057 0.2038 19.9746 -1.8249 24.4572 4 0.6982 -0.0409 -0.7716 0.6814 0.3228 0.4433 0.0166 -0.0086 0.0379 0.0841 0.0192 -0.0027 0.006 -0.0314 -0.0358 0.2174 0.0078 -0.0115 0.226 0.02 0.2096 14.6035 -0.3579 39.8796 5 0.4657 0.3192 0.3023 1.1855 -0.066 0.2824 0.0089 -0.0584 -0.0483 0.026 -0.0147 -0.0518 0.0136 -0.0069 0.0059 0.201 0.0084 -0.001 0.2118 -0.0019 0.2065 23.1149 -1.3012 37.3743 6 0.4889 1.0113 -0.404 1.3221 0.4622 1.0688 0.0088 0.027 -0.034 -0.0882 0.0316 -0.1039 -0.0662 0.1142 -0.0404 0.2027 0.0081 0.0363 0.2579 0.0044 0.2042 24.6324 6.9624 21.3382 7 0.765 0.3238 0.3426 0.9001 0.2867 1.0456 -0.0114 -0.0541 0.0145 0.0277 -0.0032 -0.0609 -0.0202 -0.0159 0.0146 0.2187 0.0025 0.002 0.1998 0.001 0.2046 22.4233 13.3881 36.6816 8 0.982 -0.0328 -0.6277 0.4192 -0.1152 1.2013 0.0256 0.0237 0.0099 0.0726 0.014 -0.0138 -0.0489 -0.0904 -0.0397 0.2246 0.0067 0.0088 0.196 0.0052 0.2031 14.0984 17.4874 36.1836 9 9.6221 3.773 -0.751 1.1558 -0.002 -0.1202 0.023 -0.1713 0.2013 -0.0225 -0.0462 0.1282 -0.0351 0.0336 0.0232 0.2301 0.0042 -0.0033 0.2105 0.0092 0.2137 16.0097 19.5537 30.669 10 3.9158 -2.243 -3.0532 3.2007 1.5275 2.3573 0.0788 -0.0547 0.0505 -0.0109 -0.0465 -0.0415 0.0403 -0.0692 -0.0323 0.201 0.0095 -0.0396 0.2047 0.0169 0.2106 2.6359 20.388 32.5312 11 -1.7639 -3.2112 -0.8133 -3.3511 2.7612 3.1988 0.4942 -0.5707 0.5576 0.0015 -0.0284 -0.0463 0.9667 -0.3466 -0.4658 0.3549 -0.2971 -0.054 0.3868 -0.0269 0.4232 -3.306 8.3072 30.1621 12 2.0254 -1.1494 -0.3146 4.8228 -0.0127 1.055 -0.0164 0.2065 0.0897 -0.2923 0.0878 0.3048 0.1196 -0.1788 -0.0714 0.1981 -0.0018 -0.0463 0.2432 0.0151 0.2047 -1.9654 17.2483 25.4422 13 -0.1913 0.2507 -0.0148 3.6534 0.8461 1.5457 -0.0084 0.0085 -0.0503 -0.1296 -0.0226 0.0442 -0.035 -0.132 0.031 0.2059 0.0065 -0.0025 0.217 -0.0014 0.1946 0.5714 2.2871 22.8498 14 3.6745 -1.3368 -1.0626 1.9926 -0.022 1.8949 0.0761 -0.1609 -0.3137 -0.067 -0.0514 0.0223 0.2834 0.0029 -0.0247 0.2458 0.0053 -0.0291 0.1743 -0.0056 0.2363 15.1928 -12.3611 27.6759 15 2.9963 -1.7272 0.0808 2.3445 -0.5921 0.7148 0.1069 0.0896 -0.0749 -0.2156 -0.0337 0.0455 0.1606 -0.0666 -0.0732 0.258 0.0024 -0.0169 0.1888 -0.029 0.2033 9.2162 -4.969 16.9316 16 0.9288 -0.8595 -1.7976 4.9177 -1.7834 1.5932 -0.0608 -0.1352 0.1832 0.3047 0.0131 -0.3634 -0.0133 0.0784 0.0477 0.2372 -0.0048 -0.0337 0.2461 -0.0281 0.2341 16.5988 2.5995 73.2768 17 2.5716 2.4323 3.487 3.3468 1.2774 5.5539 0.1497 -0.0219 -0.0689 0.0139 0.1351 -0.1864 -0.0381 -0.1109 -0.2848 0.239 0.0132 -0.0034 0.2222 0.0194 0.1832 11.6634 -6.1275 78.3317 18 0.5468 -0.262 0.3971 0.7377 -0.4936 0.8583 -0.0347 -0.0195 0.0018 0.065 0.0413 0.023 -0.0417 -0.09 -0.0065 0.2147 -0.0025 0.0076 0.2026 -0.0031 0.1954 1.3323 5.8184 63.7419 19 0.6146 0.2915 0.1347 0.3813 0.8174 1.117 -0.0146 0.0742 -0.0303 0.0639 0.0349 -0.0583 0.0574 0.0576 -0.0203 0.2283 0.0036 -0.0107 0.2253 -0.0002 0.2183 4.0768 5.5185 44.6428 20 1.6402 0.4159 0.7716 1.2238 -0.236 0.3233 -0.0648 0.1828 -0.0524 -0.1062 0.1138 0.0377 -0.0424 0.0649 -0.049 0.2306 0.0018 0.0012 0.2117 0.003 0.1946 0.6176 14.1116 51.2288 21 1.348 -0.0944 -0.598 1.3379 0.3286 1.2454 -0.035 -0.0846 0.0506 0.1196 0.0907 0.074 -0.131 -0.0751 -0.0557 0.2352 0.0077 0.0033 0.2178 -0.0066 0.1884 5.8555 13.8693 68.6986 22 1.0411 0.0986 -0.3267 0.7851 -0.3637 0.9286 -0.0299 -0.0251 0.0068 0.0123 -0.0085 -0.0303 -0.0885 0.0947 0.0384 0.2137 -0.0127 -0.0098 0.219 -0.0102 0.1823 15.5353 13.3334 58.014 23 2.3206 0.2881 0.7566 1.2967 0.8665 2.046 0.0008 0.2933 -0.0211 0.03 0.1427 -0.0472 0.0602 0.4334 -0.1435 0.19 0.0036 -0.0215 0.2833 -0.0052 0.1869 23.9757 6.2868 53.0824 24 2.4274 2.8281 0.5601 9.038 1.9587 1.9377 -0.0295 -0.0606 -0.1409 0.1396 -0.0097 -0.1318 0.1152 0.3213 0.0391 0.1929 0.0093 -0.0294 0.2696 0.026 0.1614 21.5239 5.9049 60.9693 25 -2.6027 0.9825 -7.1949 19.3443 -4.8245 3.4694 -0.6423 -1.0185 -0.6811 -1.7051 -1.473 -0.8249 0.0712 1.0623 2.1153 0.0701 0.2944 0.1654 0.3426 0.2312 0.5967 27.1479 -6.1654 56.5572 26 0.5661 0.1208 -0.3112 1.1345 -1.3376 2.7426 0.0408 0.1212 -0.1527 -0.0555 -0.0203 0.0013 0.0845 0.0986 -0.0205 0.2107 0.0332 -0.0055 0.2109 -0.009 0.2494 15.4776 -5.3664 60.0243 27 16.9483 19.9924 6.3752 13.6652 0.3971 8.7507 -0.0138 -1.4497 0.4325 -0.534 -1.6849 -0.4911 3.071 1.2679 1.6987 0.5875 0.4914 0.2307 0.0568 0.0722 0.3257 22.8433 -13.9338 62.2115 28 1.7233 -0.5157 0.6063 0.8645 -0.4066 0.5323 0.0824 0.0536 -0.0515 -0.0317 -0.0181 0.0061 0.2117 -0.0342 -0.0643 0.2557 -0.011 -0.0124 0.1882 -0.0138 0.2039 5.4104 -7.839 60.9968 29 -0.3478 -0.6425 0.513 3.4561 -0.2782 3.9571 0.0425 -0.0707 -0.1334 -0.1352 -0.0223 0.4651 0.0495 -0.2253 -0.0202 0.1517 -0.0364 0.007 0.2685 0.0232 0.2864 -11.3556 3.0591 61.0396 30 8.2456 -5.4479 6.2328 5.0383 -3.3654 6.1646 0.1128 -0.4695 -0.1526 0.1264 0.129 0.1483 0.1519 -0.3001 -0.2419 0.2475 -0.0331 0.0052 0.197 0.0296 0.1917 0.3545 -8.1936 69.9204
精密化 TLSグループ 大きな表を表示 (5 x 30) 大きな表を隠す ID Refine-ID Refine TLS-ID Auth asym-ID Auth seq-ID 1 X-RAY DIFFRACTION 1 A0 - 4 2 X-RAY DIFFRACTION 2 A5 - 21 3 X-RAY DIFFRACTION 3 A22 - 48 4 X-RAY DIFFRACTION 4 A49 - 64 5 X-RAY DIFFRACTION 5 A65 - 82 6 X-RAY DIFFRACTION 6 A83 - 97 7 X-RAY DIFFRACTION 7 A98 - 120 8 X-RAY DIFFRACTION 8 A121 - 142 9 X-RAY DIFFRACTION 9 A143 - 153 10 X-RAY DIFFRACTION 10 A154 - 173 11 X-RAY DIFFRACTION 11 A174 - 193 12 X-RAY DIFFRACTION 12 A194 - 211 13 X-RAY DIFFRACTION 13 A212 - 235 14 X-RAY DIFFRACTION 14 A236 - 250 15 X-RAY DIFFRACTION 15 A251 - 268 16 X-RAY DIFFRACTION 16 B0 - 8 17 X-RAY DIFFRACTION 17 B9 - 15 18 X-RAY DIFFRACTION 18 B16 - 52 19 X-RAY DIFFRACTION 19 B53 - 64 20 X-RAY DIFFRACTION 20 B65 - 80 21 X-RAY DIFFRACTION 21 B81 - 95 22 X-RAY DIFFRACTION 22 B96 - 127 23 X-RAY DIFFRACTION 23 B128 - 143 24 X-RAY DIFFRACTION 24 B144 - 155 25 X-RAY DIFFRACTION 25 B156 - 170 26 X-RAY DIFFRACTION 26 B171 - 180 27 X-RAY DIFFRACTION 27 B192 - 204 28 X-RAY DIFFRACTION 28 B205 - 242 29 X-RAY DIFFRACTION 29 B243 - 257 30 X-RAY DIFFRACTION 30 B258 - 268