ソフトウェア | 名称 | バージョン | 分類 |
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SBC-Collect | | データ収集 | HKL-3000 | | 位相決定 | Coot | | モデル構築 | MLPHARE | | 位相決定 | SHELX | | モデル構築 | ARP/wARP | | モデル構築 | REFMAC | 5.5.0054精密化 | HKL-3000 | | データ削減 | SCALEPACK | | データスケーリング | SHELX | | 位相決定 | |
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精密化 | 構造決定の手法: 単波長異常分散 / 解像度: 1.67→35 Å / Cor.coef. Fo:Fc: 0.974 / Cor.coef. Fo:Fc free: 0.961 / SU B: 3.133 / SU ML: 0.048 / TLS residual ADP flag: LIKELY RESIDUAL / 交差検証法: THROUGHOUT / σ(F): 2 / ESU R: 0.077 / ESU R Free: 0.081 / 立体化学のターゲット値: MAXIMUM LIKELIHOOD / 詳細: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
| Rfactor | 反射数 | %反射 | Selection details |
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Rfree | 0.17381 | 4268 | 5 % | RANDOM |
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Rwork | 0.13936 | - | - | - |
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all | 0.143 | 85080 | - | - |
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obs | 0.14104 | 80802 | 98.82 % | - |
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溶媒の処理 | イオンプローブ半径: 0.8 Å / 減衰半径: 0.8 Å / VDWプローブ半径: 1.2 Å / 溶媒モデル: MASK |
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原子変位パラメータ | Biso mean: 7.715 Å2
| Baniso -1 | Baniso -2 | Baniso -3 |
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1- | 0.21 Å2 | 0.11 Å2 | 0 Å2 |
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2- | - | 0.21 Å2 | 0 Å2 |
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3- | - | - | -0.32 Å2 |
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精密化ステップ | サイクル: LAST / 解像度: 1.67→35 Å
| タンパク質 | 核酸 | リガンド | 溶媒 | 全体 |
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原子数 | 5073 | 0 | 4 | 777 | 5854 |
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拘束条件 | Refine-ID | タイプ | Dev ideal | Dev ideal target | 数 |
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X-RAY DIFFRACTION | r_bond_refined_d0.02 | 0.022 | 5331 | X-RAY DIFFRACTION | r_bond_other_d0.001 | 0.02 | 3546 | X-RAY DIFFRACTION | r_angle_refined_deg1.502 | 1.949 | 7234 | X-RAY DIFFRACTION | r_angle_other_deg0.967 | 3 | 8705 | X-RAY DIFFRACTION | r_dihedral_angle_1_deg4.492 | 5 | 679 | X-RAY DIFFRACTION | r_dihedral_angle_2_deg38.203 | 25.362 | 276 | X-RAY DIFFRACTION | r_dihedral_angle_3_deg13.525 | 15 | 988 | X-RAY DIFFRACTION | r_dihedral_angle_4_deg19.567 | 15 | 24 | X-RAY DIFFRACTION | r_chiral_restr0.1 | 0.2 | 796 | X-RAY DIFFRACTION | r_gen_planes_refined0.008 | 0.02 | 6024 | X-RAY DIFFRACTION | r_gen_planes_other0.001 | 0.02 | 1064 | X-RAY DIFFRACTION | r_nbd_refined | | | X-RAY DIFFRACTION | r_nbd_other | | | X-RAY DIFFRACTION | r_nbtor_refined | | | X-RAY DIFFRACTION | r_nbtor_other | | | X-RAY DIFFRACTION | r_xyhbond_nbd_refined | | | X-RAY DIFFRACTION | r_xyhbond_nbd_other | | | X-RAY DIFFRACTION | r_metal_ion_refined | | | X-RAY DIFFRACTION | r_metal_ion_other | | | X-RAY DIFFRACTION | r_symmetry_vdw_refined | | | X-RAY DIFFRACTION | r_symmetry_vdw_other | | | X-RAY DIFFRACTION | r_symmetry_hbond_refined | | | X-RAY DIFFRACTION | r_symmetry_hbond_other | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_refined | | | X-RAY DIFFRACTION | r_symmetry_metal_ion_other | | | X-RAY DIFFRACTION | r_mcbond_it0.858 | 1.5 | 3209 | X-RAY DIFFRACTION | r_mcbond_other0.309 | 1.5 | 1324 | X-RAY DIFFRACTION | r_mcangle_it1.507 | 2 | 5147 | X-RAY DIFFRACTION | r_scbond_it2.755 | 3 | 2122 | X-RAY DIFFRACTION | r_scangle_it4.341 | 4.5 | 2063 | X-RAY DIFFRACTION | r_rigid_bond_restr | | | X-RAY DIFFRACTION | r_sphericity_free | | | X-RAY DIFFRACTION | r_sphericity_bonded | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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LS精密化 シェル | 解像度: 1.67→1.71 Å / Total num. of bins used: 20
| Rfactor | 反射数 | %反射 |
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Rfree | 0.25 | 285 | - |
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Rwork | 0.204 | 5642 | - |
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obs | - | - | 93.07 % |
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精密化 TLS | 手法: refined / Refine-ID: X-RAY DIFFRACTION ID | L11 (°2) | L12 (°2) | L13 (°2) | L22 (°2) | L23 (°2) | L33 (°2) | S11 (Å °) | S12 (Å °) | S13 (Å °) | S21 (Å °) | S22 (Å °) | S23 (Å °) | S31 (Å °) | S32 (Å °) | S33 (Å °) | T11 (Å2) | T12 (Å2) | T13 (Å2) | T22 (Å2) | T23 (Å2) | T33 (Å2) | Origin x (Å) | Origin y (Å) | Origin z (Å) |
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1 | 4.2898 | -0.2625 | -0.2402 | 0.202 | 1.0235 | 5.8658 | 0.1059 | 0.0182 | 0.2036 | -0.0413 | 0.0383 | -0.0224 | -0.1131 | 0.3476 | -0.1442 | 0.0515 | -0.0076 | 0.0139 | 0.0888 | -0.0104 | 0.1009 | 87.4929 | 39.8579 | 252.0368 | 2 | 1.1623 | 1.9072 | -1.9238 | 3.5756 | -2.2979 | 4.8543 | 0.0451 | -0.0615 | -0.0938 | 0.1085 | 0.006 | -0.2481 | 0.0007 | 0.2874 | -0.0511 | 0.0208 | -0.0085 | -0.0081 | 0.1085 | -0.0274 | 0.0985 | 86.5116 | 37.2067 | 262.6585 | 3 | 3.385 | 1.4082 | -1.7721 | 2.1981 | -0.7948 | 1.9775 | -0.0477 | 0.1014 | -0.1482 | 0.1187 | -0.0274 | -0.1157 | 0.0137 | 0.0183 | 0.0751 | 0.0575 | 0.0014 | -0.013 | 0.0674 | -0.0065 | 0.0716 | 74.4533 | 26.9922 | 269.838 | 4 | 3.0854 | 0.6867 | -0.044 | 0.3674 | 0.3271 | 0.5371 | -0.0217 | -0.0848 | -0.0632 | 0.0407 | -0.0156 | 0.0069 | 0.0569 | 0.029 | 0.0372 | 0.0864 | -0.0018 | 0.0115 | 0.062 | 0.0124 | 0.0839 | 61.7128 | 19.153 | 276.217 | 5 | 6.4822 | 3.5932 | -3.3903 | 4.4328 | -2.9578 | 2.7534 | 0.1319 | 0.0284 | 0.0335 | 0.1705 | -0.0442 | 0.1547 | -0.1467 | -0.0869 | -0.0877 | 0.0598 | -0.0144 | -0.0053 | 0.0777 | -0.0014 | 0.0568 | 53.4592 | 22.9706 | 275.6655 | 6 | 6.9541 | 3.1535 | -0.6928 | 2.0957 | -1.4786 | 3.3581 | -0.2207 | 0.2822 | -0.1041 | -0.0476 | 0.17 | -0.0073 | -0.0962 | -0.0479 | 0.0507 | 0.076 | -0.0275 | -0.0145 | 0.0886 | -0.0057 | 0.0502 | 64.0516 | 27.5272 | 265.8758 | 7 | 6.297 | 2.3253 | -4.4915 | 4.6741 | -5.6566 | 9.8701 | -0.0725 | 0.1851 | -0.0629 | -0.1074 | 0.0665 | 0.0824 | 0.0019 | -0.51 | 0.006 | 0.0936 | -0.0263 | -0.0076 | 0.0877 | -0.0105 | 0.0585 | 73.4685 | 29.4591 | 259.6178 | 8 | 1.4582 | 0.3639 | 0.8524 | 4.8368 | -1.7343 | 1.4972 | -0.009 | 0.0056 | 0.0309 | -0.0223 | 0.0121 | -0.2733 | 0.0836 | 0.1013 | -0.0032 | 0.0989 | 0.0212 | -0.0284 | 0.1074 | -0.0443 | 0.1236 | 82.3965 | 30.3495 | 258.0289 | 9 | 1.9164 | 0.888 | 0.5962 | 0.6896 | 1.1894 | 3.3482 | -0.0278 | -0.0381 | -0.0433 | 0.03 | 0.0025 | -0.0499 | 0.0768 | 0.0055 | 0.0252 | 0.0673 | 0.0111 | -0.0381 | 0.0749 | -0.016 | 0.1215 | 80.3727 | 19.9743 | 268.2382 | 10 | 5.3431 | 1.5922 | -2.2559 | 2.0311 | -0.5696 | 1.6846 | -0.015 | -0.2862 | -0.0139 | 0.2262 | -0.003 | -0.063 | -0.0216 | 0.1487 | 0.0179 | 0.0879 | 0.0019 | -0.0484 | 0.0727 | 0.0007 | 0.0325 | 72.1839 | 22.6968 | 279.8954 | 11 | 3.3995 | 1.7347 | -1.0526 | 1.1084 | -0.6667 | 2.4793 | 0.1046 | -0.047 | 0.0335 | 0.1764 | -0.0558 | 0.0307 | -0.1746 | -0.029 | -0.0487 | 0.1155 | 0.0027 | -0.0052 | 0.073 | 0.0082 | 0.0458 | 65.6586 | 31.1434 | 280.1463 | 12 | 3.7545 | 0.5205 | -0.0314 | 1.4114 | 1.6093 | 1.9993 | 0.1145 | -0.0491 | -0.0473 | 0.1927 | 0.0371 | -0.1811 | 0.1483 | 0.0164 | -0.1516 | 0.1239 | 0.0093 | -0.0619 | 0.099 | -0.0049 | 0.0973 | 75.1327 | 39.224 | 272.4936 | 13 | 7.662 | 3.2719 | -7.8379 | 8.5627 | -1.2113 | 8.6571 | 0.351 | -0.2079 | 0.2387 | 0.1876 | 0.0177 | -0.2084 | -0.3798 | 0.2573 | -0.3687 | 0.0788 | -0.0383 | -0.0008 | 0.0824 | -0.0189 | 0.0997 | 81.0397 | 45.2462 | 265.8512 | 14 | 1.046 | -0.232 | -1.4783 | 0.214 | 0.1024 | 2.4208 | 0.0096 | 0.0324 | 0.0046 | 0.0236 | 0.0095 | -0.0163 | -0.065 | -0.0532 | -0.0191 | 0.0709 | -0.0079 | -0.0043 | 0.0785 | -0.0086 | 0.0733 | 70.7406 | 41.0947 | 264.2702 | 15 | 4.0062 | 2.4384 | -2.563 | 5.9028 | -2.1184 | 4.1547 | 0.0296 | -0.2016 | 0.0997 | 0.1333 | 0.0498 | 0.1081 | -0.174 | -0.0016 | -0.0794 | 0.0771 | 0.0133 | -0.0061 | 0.0686 | -0.0038 | 0.029 | 57.6688 | 36.4631 | 279.8003 | 16 | 2.2738 | -2.8045 | 1.2117 | 3.5028 | -1.4623 | 0.6719 | -0.1224 | -0.0477 | 0.1526 | 0.1401 | 0.0446 | -0.1982 | -0.0983 | -0.0342 | 0.0778 | 0.1422 | 0.01 | 0.0183 | 0.0924 | 0.0259 | 0.0847 | 39.4408 | 53.0088 | 210.1681 | 17 | 3.7628 | 1.9629 | 1.8941 | 3.4039 | -0.6714 | 2.7402 | -0.0926 | 0.2054 | 0.1289 | -0.1396 | 0.1167 | 0.0583 | 0.0214 | 0.0205 | -0.0241 | 0.0931 | 0.0096 | 0.0012 | 0.0754 | 0.0263 | 0.0523 | 38.9309 | 44.4403 | 208.7753 | 18 | 5.7485 | 1.4188 | -1.5107 | 2.3274 | -1.8605 | 1.9392 | 0.0444 | 0.2975 | -0.0129 | -0.0658 | 0.0352 | 0.0565 | -0.1218 | -0.1681 | -0.0797 | 0.0933 | 0.0171 | 0.0032 | 0.0981 | 0.0132 | 0.0581 | 30.4397 | 38.0962 | 211.5428 | 19 | 1.6346 | 0.798 | -1.2879 | 1.5876 | -1.9035 | 2.4814 | -0.0084 | 0.0346 | 0.021 | 0.1618 | 0.0436 | 0.085 | -0.1327 | -0.0345 | -0.0352 | 0.0729 | 0.0054 | 0.0113 | 0.0626 | -0.007 | 0.0585 | 22.8691 | 28.6248 | 226.3177 | 20 | 2.2411 | 1.1562 | -0.6486 | 2.1498 | -1.704 | 2.6784 | -0.0507 | -0.0019 | -0.1827 | -0.0192 | 0.0742 | 0.1091 | 0.152 | -0.0482 | -0.0235 | 0.0845 | -0.0107 | 0.0172 | 0.0746 | -0.0052 | 0.0537 | 18.7034 | 15.8735 | 237.8386 | 21 | 2.2084 | 1.7038 | -2.0856 | 3.8078 | -2.3633 | 3.2795 | -0.0242 | 0.028 | -0.1361 | 0.2022 | 0.1028 | -0.0959 | -0.119 | 0.0695 | -0.0786 | 0.0697 | -0.0071 | -0.0043 | 0.0838 | -0.0006 | 0.0625 | 27.3105 | 22.3668 | 233.3969 | 22 | 3.1413 | 1.0329 | 1.6772 | 10.7761 | -2.4989 | 2.5053 | 0.0201 | -0.2963 | 0.0696 | 0.2849 | -0.0123 | -0.0466 | -0.0576 | 0.0503 | -0.0078 | 0.1054 | -0.011 | -0.008 | 0.2027 | -0.0175 | 0.0617 | 33.1147 | 33.0088 | 227.1632 | 23 | 5.4239 | 0.1176 | -0.9517 | 0.8671 | 0.1676 | 1.5171 | 0.071 | -0.157 | 0.2889 | -0.0706 | -0.1306 | 0.073 | -0.0739 | -0.0599 | 0.0596 | 0.0682 | -0.0167 | 0.0012 | 0.0912 | -0.029 | 0.0752 | 33.4773 | 42.1803 | 219.3233 | 24 | 1.879 | 0.9094 | 0.4522 | 3.3621 | 3.0861 | 4.0255 | -0.025 | 0.1828 | 0.071 | -0.1275 | -0.0048 | 0.1021 | -0.1821 | -0.216 | 0.0298 | 0.0601 | 0.0247 | -0.0155 | 0.0836 | 0.0112 | 0.0463 | 19.1147 | 39.0368 | 220.9696 | 25 | 1.6614 | 0.2661 | -0.6485 | 2.9562 | -2.5657 | 2.3945 | -0.0322 | 0.1249 | -0.0747 | -0.1651 | 0.0684 | 0.1633 | 0.1714 | -0.1043 | -0.0362 | 0.0666 | -0.0277 | 0.0018 | 0.1024 | -0.0295 | 0.1103 | 14.9058 | 22.9954 | 224.7854 | 26 | 2.1523 | 1.1685 | -0.6161 | 1.4508 | -1.2941 | 2.8474 | -0.0502 | 0.1205 | -0.1831 | -0.0546 | 0.0206 | -0.0593 | 0.1192 | -0.1192 | 0.0297 | 0.0472 | -0.0143 | 0.0012 | 0.0795 | -0.0149 | 0.0768 | 22.8745 | 18.5466 | 221.902 | 27 | 1.5034 | 2.1504 | 0.0208 | 5.0399 | -0.9757 | 3.4848 | -0.0355 | 0.1511 | -0.0681 | -0.2035 | 0.0716 | -0.0565 | -0.0141 | -0.2598 | -0.0361 | 0.0554 | 0.0128 | -0.0021 | 0.0984 | -0.0011 | 0.0389 | 33.8634 | 28.0798 | 210.475 | 28 | 2.8096 | 1.2382 | 0.0014 | 5.5532 | 6.0145 | 9.4914 | -0.0787 | 0.212 | -0.097 | -0.4454 | 0.1777 | -0.0436 | -0.3482 | -0.0703 | -0.099 | 0.0893 | -0.0259 | 0.0157 | 0.0908 | 0.0106 | 0.0425 | 42.5806 | 35.1913 | 208.8769 | 29 | 0.7969 | 1.0489 | -0.3998 | 3.3959 | -0.6008 | 0.4986 | 0.022 | 0.0255 | -0.0589 | 0.0798 | -0.0337 | -0.0712 | -0.0145 | 0.0062 | 0.0117 | 0.0583 | -0.0075 | -0.0039 | 0.0786 | -0.0004 | 0.0631 | 37.3669 | 24.617 | 219.4686 | 30 | 7.0414 | 1.5035 | -3.5833 | 4.5249 | -0.6642 | 4.1501 | -0.104 | 0.0909 | -0.3296 | -0.1782 | 0.134 | -0.0687 | 0.1851 | 0.0383 | -0.03 | 0.0398 | -0.0132 | -0.005 | 0.0656 | -0.0053 | 0.0661 | 28.1219 | 10.2051 | 224.8557 | 31 | 3.9797 | -0.9595 | 0.3779 | 3.482 | -2.1254 | 2.3402 | 0.055 | -0.118 | -0.1417 | -0.0431 | 0.11 | 0.4283 | 0.2253 | -0.192 | -0.165 | 0.0508 | -0.0358 | 0.0112 | 0.0954 | 0.0013 | 0.149 | 2.6725 | 22.3594 | 250.6344 | 32 | 0.9854 | -0.0464 | -0.1011 | 2.009 | -1.8461 | 2.8452 | -0.056 | 0.0978 | -0.0975 | -0.1305 | 0.0874 | 0.1671 | 0.0871 | -0.267 | -0.0314 | 0.0265 | -0.0047 | 0.0155 | 0.0972 | -0.0195 | 0.115 | 4.2695 | 33.0743 | 244.8841 | 33 | 3.3695 | 2.1568 | -0.973 | 1.4354 | -0.4229 | 2.1131 | -0.0543 | 0.0973 | -0.1342 | -0.0853 | 0.046 | -0.0618 | -0.065 | -0.0182 | 0.0083 | 0.075 | 0.013 | -0.0029 | 0.0728 | -0.0063 | 0.0764 | 19.3636 | 41.051 | 234.5092 | 34 | 5.7609 | 3.6307 | 0.6847 | 3.1317 | -0.2006 | 0.715 | -0.0626 | 0.0233 | 0.0596 | -0.1857 | 0.0361 | -0.0666 | 0.057 | -0.1739 | 0.0265 | 0.1066 | 0.0094 | 0.0358 | 0.1786 | 0.012 | 0.0813 | 32.523 | 47.9961 | 227.4113 | 35 | 9.4422 | 0.7851 | -0.1839 | 3.5596 | -4.9573 | 6.9934 | 0.275 | -0.2455 | 0.3089 | 0.3065 | -0.1688 | 0.0954 | -0.4018 | 0.2142 | -0.1062 | 0.0794 | 0.013 | 0.0352 | 0.0805 | -0.0064 | 0.0741 | 39.096 | 52.5017 | 232.6481 | 36 | 2.6249 | 3.3038 | -1.7429 | 4.5512 | -1.2841 | 3.5625 | 0.0357 | 0.0451 | -0.1575 | 0.1125 | 0.0553 | -0.243 | -0.0841 | 0.0669 | -0.0909 | 0.0952 | -0.006 | 0.0128 | 0.0888 | 0.0068 | 0.1024 | 32.4341 | 44.6989 | 236.4542 | 37 | 10.6331 | 3.7212 | -5.674 | 4.5273 | -1.6546 | 3.0636 | -0.2533 | -0.1362 | -0.5338 | -0.1488 | -0.0238 | -0.1096 | 0.1187 | 0.0682 | 0.277 | 0.0707 | 0.0374 | 0.0271 | 0.0899 | 0.0382 | 0.1279 | 25.4856 | 36.8582 | 240.5949 | 38 | 9.8431 | 5.3077 | -5.8493 | 3.2644 | -4.3663 | 7.1515 | 0.0373 | -0.0312 | -0.1715 | -0.0022 | -0.064 | -0.0934 | 0.0398 | 0.1114 | 0.0267 | 0.0953 | 0.0444 | 0.0684 | 0.06 | 0.0342 | 0.1921 | 19.3536 | 30.8081 | 241.6845 | 39 | 1.3729 | 0.1744 | 0.0677 | 1.0213 | -1.4464 | 5.7224 | 0.0128 | -0.0313 | -0.0232 | -0.184 | -0.0832 | 0.0899 | 0.2708 | -0.1083 | 0.0704 | 0.1004 | 0.021 | 0.014 | 0.0664 | -0.0056 | 0.0824 | 10.7218 | 27.3444 | 241.4752 | 40 | 1.3593 | -2.2225 | -0.9285 | 5.5756 | 2.168 | 1.8931 | 0.0461 | 0.082 | -0.0179 | -0.0914 | -0.0544 | 0.2406 | -0.049 | -0.2293 | 0.0083 | 0.0358 | 0.0271 | -0.0148 | 0.1144 | 0.004 | 0.0798 | 11.9144 | 35.7728 | 229.3838 | 41 | 2.7918 | 1.1608 | -0.9806 | 1.3313 | 0.1389 | 1.4612 | -0.0084 | 0.0444 | 0.1215 | -0.1 | 0.0437 | 0.1379 | -0.1801 | -0.0904 | -0.0353 | 0.0969 | 0.0401 | -0.0087 | 0.0527 | 0.0274 | 0.0659 | 20.6859 | 50.2166 | 228.9107 | 42 | 2.6694 | 1.9523 | -1.5486 | 2.1657 | -1.5883 | 2.1367 | 0.0107 | 0.0081 | 0.0846 | 0.036 | -0.0218 | 0.0918 | -0.2191 | -0.0843 | 0.0112 | 0.0731 | 0.0206 | 0.0009 | 0.0688 | 0.0098 | 0.0778 | 19.4479 | 50.2992 | 239.9791 | 43 | 3.3555 | 1.6569 | -1.525 | 8.6118 | -2.4073 | 1.9072 | 0.0568 | -0.1634 | 0.1009 | 0.1554 | -0.127 | 0.4974 | -0.0282 | -0.058 | 0.0701 | 0.0286 | -0.0006 | 0.039 | 0.1151 | -0.0301 | 0.1037 | 7.1286 | 40.0358 | 252.2705 | 44 | 1.0386 | 1.6336 | -0.3793 | 2.8195 | -0.2441 | 0.7026 | 0.0218 | 0.0007 | -0.0458 | 0.0632 | -0.0442 | -0.0398 | -0.0423 | -0.0658 | 0.0224 | 0.0626 | 0.0098 | 0.0176 | 0.0743 | 0.0053 | 0.0898 | 17.1785 | 38.4003 | 251.7544 | 45 | 3.6301 | 3.8992 | -2.2453 | 5.6098 | -3.3773 | 6.2619 | -0.0128 | 0.0387 | 0.1445 | 0.1373 | 0.0738 | 0.1572 | -0.1406 | -0.0293 | -0.061 | 0.0609 | 0.0226 | 0.0057 | 0.0466 | 0.0066 | 0.0564 | 27.7721 | 54.5776 | 245.1925 | 46 | 0.0252 | 0.0796 | -0.1178 | 0.2775 | -0.4224 | 0.6494 | 0.003 | 0.0004 | 0.0207 | 0.0363 | 0.0151 | 0.0203 | -0.0637 | -0.0486 | -0.0182 | 0.1435 | 0.0067 | -0.0038 | 0.1102 | 0.0057 | 0.114 | 54.4934 | 1.1778 | 286.7443 | 47 | 8.1305 | -1.3726 | 0.0722 | 2.182 | -2.1427 | 2.7226 | 0.0406 | -0.2523 | -0.2377 | -0.0227 | -0.1184 | -0.0191 | 0.081 | 0.1237 | 0.0779 | 0.0974 | -0.0054 | -0.0081 | 0.076 | 0.0126 | 0.0304 | 57.8378 | -2.2741 | 279.4356 | 48 | 1.5911 | 1.5533 | -1.5516 | 1.9227 | -1.3699 | 2.3433 | 0.0342 | -0.0706 | -0.0627 | 0.1337 | -0.0342 | -0.1024 | -0.1008 | 0.0146 | 0 | 0.07 | 0.0036 | -0.0084 | 0.0658 | 0.0086 | 0.0661 | 70.2978 | 6.9452 | 268.1891 | 49 | 1.1947 | -1.0268 | 0.3881 | 2.5601 | -0.7356 | 0.9386 | 0.0037 | -0.1272 | 0.0834 | 0.1158 | -0.035 | -0.0815 | -0.0356 | 0.1028 | 0.0313 | 0.0931 | -0.0288 | 0.0007 | 0.0688 | -0.015 | 0.0758 | 78.0543 | 20.733 | 254.5718 | 50 | 9.9589 | -0.7476 | -2.8084 | 4.6054 | -2.6299 | 6.0811 | -0.1648 | 0.368 | -0.3208 | -0.3079 | 0.0782 | -0.1163 | 0.3196 | -0.043 | 0.0866 | 0.1007 | -0.0064 | 0.0011 | 0.0649 | -0.0059 | 0.078 | 77.567 | 21.1585 | 243.2847 | 51 | 2.1654 | 1.6996 | -3.0388 | 2.784 | -3.1755 | 6.5823 | 0.0406 | 0.132 | -0.1471 | 0.0817 | 0.086 | 0.1343 | -0.2616 | -0.1318 | -0.1266 | 0.0659 | 0.0063 | 0.0071 | 0.0793 | 0.0141 | 0.0962 | 69.5942 | 17.0489 | 252.9403 | 52 | 3.7469 | -1.7579 | -3.2968 | 1.5648 | 0.097 | 11.5682 | 0.1443 | 0.1814 | 0.2748 | -0.0811 | -0.0279 | 0.1748 | -0.1686 | -0.3081 | -0.1164 | 0.1052 | 0.0138 | -0.0206 | 0.0886 | 0.0565 | 0.274 | 62.1825 | 12.4718 | 263.8389 | 53 | 5.3003 | 1.3016 | 0.8818 | 2.7963 | -0.1489 | 1.3716 | 0.0715 | -0.2038 | 0.2981 | 0.0821 | 0.0483 | -0.0495 | -0.0219 | -0.0171 | -0.1198 | 0.0645 | -0.0006 | 0.0217 | 0.0658 | -0.0148 | 0.1149 | 60.1063 | 7.5095 | 274.6119 | 54 | 3.8876 | -0.2033 | -2.036 | 3.4539 | 1.6385 | 1.7525 | -0.017 | -0.0694 | -0.1761 | 0.1611 | -0.0443 | -0.0176 | 0.0596 | 0.0302 | 0.0614 | 0.1016 | 0.0123 | -0.0295 | 0.0836 | -0.0021 | 0.0763 | 72.759 | 13.3717 | 274.3816 | 55 | 1.4616 | 1.4589 | -2.3619 | 2.0995 | -2.6089 | 5.8098 | -0.0532 | -0.0158 | -0.2174 | 0.0781 | -0.0092 | -0.2598 | -0.0028 | 0.1169 | 0.0624 | 0.0447 | 0.0183 | -0.0137 | 0.0754 | -0.0024 | 0.1272 | 81.6709 | 11.206 | 263.3037 | 56 | 3.7405 | 2.8496 | -2.6183 | 3.7167 | -3.2853 | 3.8115 | -0.0879 | 0.0762 | -0.1858 | -0.0534 | 0.0307 | -0.2437 | 0.1046 | 0.0991 | 0.0572 | 0.044 | -0.0021 | 0.0076 | 0.0788 | -0.0141 | 0.0746 | 78.3434 | 7.8103 | 252.807 | 57 | 1.8298 | -0.1295 | -1.9302 | 1.0009 | -0.5627 | 3.6218 | -0.083 | 0.0279 | -0.1009 | -0.0455 | -0.0099 | -0.1195 | 0.2155 | 0.0274 | 0.0929 | 0.078 | 0.0053 | -0.0098 | 0.0509 | 0.0182 | 0.0798 | 66.73 | -3.5865 | 264.1532 | 58 | 5.3939 | -3.9656 | 0.1354 | 9.9579 | 0.0402 | 3.2304 | -0.1233 | 0.0157 | -0.3764 | 0.2502 | 0.0764 | -0.0215 | 0.2781 | 0.1061 | 0.0468 | 0.0826 | -0.0144 | 0.0181 | 0.0703 | 0.0085 | 0.0918 | 56.657 | -6.2696 | 269.9297 | 59 | 0.7135 | 0.0358 | -1.3673 | 0.5498 | 0.0942 | 2.8376 | 0.0332 | 0.0816 | 0.0327 | 0.0141 | 0.0496 | 0.0084 | -0.02 | -0.1034 | -0.0828 | 0.0586 | -0.0034 | -0.0014 | 0.0665 | 0.0169 | 0.0755 | 62.2032 | 2.1693 | 257.6842 | 60 | 9.3859 | 4.9687 | -3.1295 | 5.8101 | -0.5468 | 6.932 | -0.0677 | 0.0639 | -0.2742 | -0.1317 | 0.0027 | -0.1 | 0.2563 | 0.1935 | 0.0651 | 0.0362 | 0.0102 | 0.0025 | 0.0594 | -0.0049 | 0.058 | 73.8458 | 5.3755 | 244.4438 |
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精密化 TLSグループ | ID | Refine-ID | Refine TLS-ID | Auth asym-ID | Auth seq-ID |
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1 | X-RAY DIFFRACTION | 1 | A3 - 10 | 2 | X-RAY DIFFRACTION | 2 | A11 - 20 | 3 | X-RAY DIFFRACTION | 3 | A21 - 32 | 4 | X-RAY DIFFRACTION | 4 | A33 - 43 | 5 | X-RAY DIFFRACTION | 5 | A44 - 54 | 6 | X-RAY DIFFRACTION | 6 | A55 - 63 | 7 | X-RAY DIFFRACTION | 7 | A64 - 69 | 8 | X-RAY DIFFRACTION | 8 | A70 - 79 | 9 | X-RAY DIFFRACTION | 9 | A80 - 86 | 10 | X-RAY DIFFRACTION | 10 | A87 - 99 | 11 | X-RAY DIFFRACTION | 11 | A100 - 113 | 12 | X-RAY DIFFRACTION | 12 | A114 - 120 | 13 | X-RAY DIFFRACTION | 13 | A121 - 127 | 14 | X-RAY DIFFRACTION | 14 | A128 - 147 | 15 | X-RAY DIFFRACTION | 15 | A148 - 156 | 16 | X-RAY DIFFRACTION | 16 | B-2 - 5 | 17 | X-RAY DIFFRACTION | 17 | B6 - 14 | 18 | X-RAY DIFFRACTION | 18 | B15 - 22 | 19 | X-RAY DIFFRACTION | 19 | B23 - 38 | 20 | X-RAY DIFFRACTION | 20 | B39 - 48 | 21 | X-RAY DIFFRACTION | 21 | B49 - 60 | 22 | X-RAY DIFFRACTION | 22 | B61 - 66 | 23 | X-RAY DIFFRACTION | 23 | B67 - 79 | 24 | X-RAY DIFFRACTION | 24 | B80 - 89 | 25 | X-RAY DIFFRACTION | 25 | B90 - 100 | 26 | X-RAY DIFFRACTION | 26 | B101 - 114 | 27 | X-RAY DIFFRACTION | 27 | B115 - 126 | 28 | X-RAY DIFFRACTION | 28 | B127 - 132 | 29 | X-RAY DIFFRACTION | 29 | B133 - 148 | 30 | X-RAY DIFFRACTION | 30 | B149 - 156 | 31 | X-RAY DIFFRACTION | 31 | C0 - 11 | 32 | X-RAY DIFFRACTION | 32 | C12 - 20 | 33 | X-RAY DIFFRACTION | 33 | C21 - 37 | 34 | X-RAY DIFFRACTION | 34 | C38 - 43 | 35 | X-RAY DIFFRACTION | 35 | C44 - 48 | 36 | X-RAY DIFFRACTION | 36 | C49 - 57 | 37 | X-RAY DIFFRACTION | 37 | C58 - 63 | 38 | X-RAY DIFFRACTION | 38 | C64 - 69 | 39 | X-RAY DIFFRACTION | 39 | C70 - 79 | 40 | X-RAY DIFFRACTION | 40 | C80 - 89 | 41 | X-RAY DIFFRACTION | 41 | C90 - 100 | 42 | X-RAY DIFFRACTION | 42 | C101 - 118 | 43 | X-RAY DIFFRACTION | 43 | C119 - 128 | 44 | X-RAY DIFFRACTION | 44 | C129 - 145 | 45 | X-RAY DIFFRACTION | 45 | C146 - 156 | 46 | X-RAY DIFFRACTION | 46 | D-2 - 5 | 47 | X-RAY DIFFRACTION | 47 | D6 - 14 | 48 | X-RAY DIFFRACTION | 48 | D15 - 34 | 49 | X-RAY DIFFRACTION | 49 | D35 - 42 | 50 | X-RAY DIFFRACTION | 50 | D43 - 48 | 51 | X-RAY DIFFRACTION | 51 | D49 - 60 | 52 | X-RAY DIFFRACTION | 52 | D61 - 66 | 53 | X-RAY DIFFRACTION | 53 | D67 - 77 | 54 | X-RAY DIFFRACTION | 54 | D78 - 86 | 55 | X-RAY DIFFRACTION | 55 | D87 - 98 | 56 | X-RAY DIFFRACTION | 56 | D99 - 113 | 57 | X-RAY DIFFRACTION | 57 | D114 - 125 | 58 | X-RAY DIFFRACTION | 58 | D126 - 132 | 59 | X-RAY DIFFRACTION | 59 | D133 - 148 | 60 | X-RAY DIFFRACTION | 60 | D149 - 156 | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | | |
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