SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW ... SHEET DETERMINATION METHOD: DSSP THE SHEETS PRESENTED AS "AA" IN EACH CHAIN ON SHEET RECORDS BELOW IS ACTUALLY AN 8-STRANDED BARREL THIS IS REPRESENTED BY A 9-STRANDED SHEET IN WHICH THE FIRST AND LAST STRANDS ARE IDENTICAL.
Mass: 18.015 Da / Num. of mol.: 693 / Source method: isolated from a natural source / Formula: H2O
Nonpolymer details
GALACTOSE (GAL): GALACTOSE IS PART OF A PENTASACCHARIDE GAL-MAN4 MANNOSE (MAN): THE FOUR MANNOSE ...GALACTOSE (GAL): GALACTOSE IS PART OF A PENTASACCHARIDE GAL-MAN4 MANNOSE (MAN): THE FOUR MANNOSE GROUPS ARE PART OF A PENTASACCHARIDE GAL-MAN4
Sequence details
STARTING RESIDUE IS LEU 53
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Experimental details
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Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
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Sample preparation
Crystal
Density Matthews: 2.37 Å3/Da / Density % sol: 59.37 % / Description: NONE
Resolution: 1.57→10.53 Å / Cor.coef. Fo:Fc: 0.98 / Cor.coef. Fo:Fc free: 0.971 / SU B: 1.479 / SU ML: 0.025 / Cross valid method: THROUGHOUT / ESU R: 0.058 / ESU R Free: 0.051 / Stereochemistry target values: MAXIMUM LIKELIHOOD Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS. U VALUES REFINED INDIVIDUALLY
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.13672
3652
5 %
RANDOM
Rwork
0.10861
-
-
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obs
0.11002
68731
99.65 %
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Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK