Mass: 16031.430 Da / Num. of mol.: 1 Source method: isolated from a genetically manipulated source Source: (gene. exp.) artificial gene (others) / Production host: Escherichia coli (E. coli)
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Experimental details
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Experiment
Experiment
Method: SOLUTION NMR
NMR experiment
Conditions-ID
Experiment-ID
Solution-ID
Type
1
1
1
2D 1H-15N HSQC
1
2
2
2D 1H-13C HSQC
1
3
1
3D HNCO
1
4
1
3DCBCA(CO)NH
1
5
1
3D HN(CA)CB
1
6
1
3D 1H-13C arom NOESY
1
7
1
3D simutaneous 13C-aromatic,13C-aliphatic,15N edited 1H-1H NOESY
1
8
3
2D 1H-15N HSQC
1
9
2
2DHetNOE
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Sample preparation
Details
Solution-ID
Contents
Solvent system
1
0.71 mM [U-100% 13C; U-100% 15N] OR36, 90% H2O/10% D2O
90% H2O/10% D2O
2
0.95 mM [U-10% 13C; U-100% 15N] OR36, 90% H2O/10% D2O
90% H2O/10% D2O
3
0.95 mM [U-10% 13C; U-100% 15N] OR36, 90% H2O/10% D2O