+Open data
-Basic information
Entry | Database: PDB / ID: 2km9 | ||||||
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Title | Omega conotoxin-FVIA | ||||||
Components | omega_conotoxin-FVIA | ||||||
Keywords | NEUROPEPTIDE / omega conotoxin / FVIA | ||||||
Method | SOLUTION NMR / simulated annealing | ||||||
Model details | lowest energy, model 1 | ||||||
Authors | Lee, S. / Kim, J. / Lee, J. / Jung, H. | ||||||
Citation | Journal: To be Published Title: Structure of omega conotoxin-FVIA Authors: Lee, S. / Lee, J. / Jung, H. / Kim, J. | ||||||
History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 2km9.cif.gz | 118.8 KB | Display | PDBx/mmCIF format |
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PDB format | pdb2km9.ent.gz | 94.1 KB | Display | PDB format |
PDBx/mmJSON format | 2km9.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Summary document | 2km9_validation.pdf.gz | 336.5 KB | Display | wwPDB validaton report |
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Full document | 2km9_full_validation.pdf.gz | 440 KB | Display | |
Data in XML | 2km9_validation.xml.gz | 11.2 KB | Display | |
Data in CIF | 2km9_validation.cif.gz | 17.9 KB | Display | |
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/km/2km9 ftp://data.pdbj.org/pub/pdb/validation_reports/km/2km9 | HTTPS FTP |
-Related structure data
Related structure data | |
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Similar structure data |
-Links
-Assembly
Deposited unit |
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1 |
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NMR ensembles |
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-Components
#1: Protein/peptide | Mass: 2579.037 Da / Num. of mol.: 1 / Source method: obtained synthetically / Details: Peptide synthesis |
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-Experimental details
-Experiment
Experiment | Method: SOLUTION NMR | ||||||||||||||||||||
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NMR experiment |
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-Sample preparation
Details | Contents: 7mM omega conotoxin-FVIA-1, 90% H2O/10% D2O / Solvent system: 90% H2O/10% D2O |
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Sample | Conc.: 7 mM / Component: omega conotoxin-FVIA-1 |
Sample conditions | pH: 3.5 / Pressure: ambient / Temperature: 298 K |
-NMR measurement
NMR spectrometer | Type: Bruker Avance / Manufacturer: Bruker / Model: Avance / Field strength: 600 MHz |
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-Processing
NMR software | Name: X-PLOR / Developer: Brunger A. T. et.al. / Classification: refinement |
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Refinement | Method: simulated annealing / Software ordinal: 1 |
NMR representative | Selection criteria: lowest energy |
NMR ensemble | Conformer selection criteria: structures with the lowest energy Conformers calculated total number: 100 / Conformers submitted total number: 20 / Representative conformer: 1 |