タイプ: Cyclic peptide / クラス: 抗菌剤 / 分子量: 1031.236 Da / 分子数: 1 / 由来タイプ: 合成 詳細: Synthesis of the linear peptide by the solid-phase method using standard Fmoc chemistry in continuous flow mode (MilliGen 9050 peptide synthesizer; Millipore, USA). Cyclization manually by ...詳細: Synthesis of the linear peptide by the solid-phase method using standard Fmoc chemistry in continuous flow mode (MilliGen 9050 peptide synthesizer; Millipore, USA). Cyclization manually by applying HAPyU-chemistry. Purification by RP-HPLC (Shimadzu LC-10AD system), Characterization by matrix-assisted laser desorption mass spectrometry (MALDI II, Kratos, Manchester, UK). 参照: CYCLIC HEXAPEPTIDE RR(NAL)(NAL)RF
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実験情報
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実験
実験
手法: 溶液NMR
NMR実験
Conditions-ID
Experiment-ID
Solution-ID
タイプ
1
1
1
2D NOESY
1
2
1
2D TOCSY
1
3
1
DQF-COSY
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試料調製
詳細
内容: 2.5 mM c-RY, 50 mM D38 dodecyl phosphocholine / 溶媒系: 90% H2O/10% D2O
試料状態
pH: 6.3 / 圧: ambient / 温度: 300 K
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NMR測定
NMRスペクトロメーター
タイプ: Bruker DRX / 製造業者: Bruker / モデル: DRX / 磁場強度: 600 MHz