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- PDB-1i0n: 1.3 A STRUCTURE OF THE A-DECAMER GCGTATACGC WITH A SINGLE 2'-O-ME... -
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Open data
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Basic information
Entry | Database: PDB / ID: 1i0n | ||||||||||||||||||
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Title | 1.3 A STRUCTURE OF THE A-DECAMER GCGTATACGC WITH A SINGLE 2'-O-METHYL-[TRI(OXYETHYL)] THYMINE IN PLACE OF T6, MEDIUM RB-SALT | ||||||||||||||||||
![]() | 5'-D(*![]() DNA / A-form double helix / modified sugar | Function / homology | RUBIDIUM ION / DNA | ![]() Method | ![]() ![]() ![]() ![]() Tereshko, V. / Wilds, C.J. / Minasov, G. / Prakash, T.P. / Maier, M.A. / Howard, A. / Wawrzak, Z. / Manoharan, M. / Egli, M. | ![]() ![]() Title: Detection of alkali metal ions in DNA crystals using state-of-the-art X-ray diffraction experiments. Authors: Tereshko, V. / Wilds, C.J. / Minasov, G. / Prakash, T.P. / Maier, M.A. / Howard, A. / Wawrzak, Z. / Manoharan, M. / Egli, M. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 26.7 KB | Display | ![]() |
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PDB format | ![]() | 17.1 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Summary document | ![]() | 367.4 KB | Display | ![]() |
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Full document | ![]() | 381.5 KB | Display | |
Data in XML | ![]() | 4.9 KB | Display | |
Data in CIF | ![]() | 6.5 KB | Display | |
Arichive directory | ![]() ![]() | HTTPS FTP |
-Related structure data
Related structure data | ![]() 1i0fC ![]() 1i0gC ![]() 1i0jC ![]() 1i0kC ![]() 1i0mC ![]() 1i0oC ![]() 1i0pC ![]() 1i0qC ![]() 1i0tC C: citing same article ( |
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Similar structure data |
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Links
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Assembly
Deposited unit | ![]()
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Unit cell |
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Components
#1: DNA chain | Mass: 3207.189 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Chemical | #3: Water | ChemComp-HOH / | |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 1.89 Å3/Da / Density % sol: 35.08 % | ||||||||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 298 K / Method: vapor diffusion, hanging drop / pH: 6 Details: Rb salt, pH 6.0, VAPOR DIFFUSION, HANGING DROP at 298 K | ||||||||||||||||||||||||||||||||||||||||||
Crystal grow | *PLUS | ||||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 100 K |
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Diffraction source | Source: ![]() ![]() ![]() |
Detector | Type: MARRESEARCH / Detector: CCD / Date: Nov 1, 1999 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength: 0.95 Å / Relative weight: 1 |
Reflection | Resolution: 1.3→20 Å / Num. all: 12230 / Num. obs: 12230 / % possible obs: 99.5 % / Observed criterion σ(F): 0 / Observed criterion σ(I): 0 / Rmerge(I) obs: 0.044 |
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Processing
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Refinement | Method to determine structure: ![]()
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Refinement step | Cycle: LAST / Resolution: 1.3→20 Å
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Software | *PLUS Name: SHELXL-97 / Classification: refinement | ||||||||||||||||||||
Refine LS restraints | *PLUS
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