Mass: 1195.408 Da / Num. of mol.: 1 / Fragment: REACTIVE SITE LOOP I / Source method: obtained synthetically / Source: (synth.) synthetic construct (others)
Compound details
DETAILS ABOUT PEPTIDE DESIGN ARE DESCRIBED IN REFERENCE 1
-
Experimental details
-
Experiment
Experiment
Method: SOLUTION NMR
NMR experiment
Conditions-ID
Experiment-ID
Solution-ID
Type
1
1
1
TOCSY
1
2
1
COSY
1
3
1
NOESY
1
4
1
ROESY
NMR details
Text: THE STRUCTURE WAS DETERMINED USING 1H-NMR. THE PAIRWISE RMSD FOR FAMILY OF 30 STRUCTURES IS 0.61+/ -0.19A FOR THE BACKBONE ATOMS AND 1.94+/-0.51A FOR ALL HEAVY ATOMS.
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Sample preparation
Sample conditions
pH: 3.8 / Temperature: 298 K
Crystal grow
*PLUS
Method: other / Details: NMR
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NMR measurement
NMR spectrometer
Type: Bruker AMX / Manufacturer: Bruker / Model: AMX / Field strength: 600 MHz
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