+Open data
-Basic information
Entry | Database: PDB / ID: 1d82 | ||||||||||||||||||
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Title | CRYSTAL AND MOLECULAR STRUCTURE OF D(GTCTAGAC) | ||||||||||||||||||
Components | DNA (5'-D(*Keywords | DNA / A-DNA / DOUBLE HELIX | Function / homology | DNA | Function and homology information Method | X-RAY DIFFRACTION / Resolution: 2.5 Å | Authors | Cervi, A. / Langlois D'Estaintot, B. / Hunter, W.N. | Citation | Journal: Acta Crystallogr.,Sect.B / Year: 1992 | Title: Crystal and Molecular Structure of d(GTCTAGAC) Authors: Cervi, A. / Langlois D'Estaintot, B. / Hunter, W.N. History |
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-Structure visualization
Structure viewer | Molecule: MolmilJmol/JSmol |
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-Downloads & links
-Download
PDBx/mmCIF format | 1d82.cif.gz | 12.6 KB | Display | PDBx/mmCIF format |
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PDB format | pdb1d82.ent.gz | 7.1 KB | Display | PDB format |
PDBx/mmJSON format | 1d82.json.gz | Tree view | PDBx/mmJSON format | |
Others | Other downloads |
-Validation report
Arichive directory | https://data.pdbj.org/pub/pdb/validation_reports/d8/1d82 ftp://data.pdbj.org/pub/pdb/validation_reports/d8/1d82 | HTTPS FTP |
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-Related structure data
Similar structure data |
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-Links
-Assembly
Deposited unit |
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1 |
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Unit cell |
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-Components
#1: DNA chain | Mass: 2426.617 Da / Num. of mol.: 1 / Source method: obtained synthetically |
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#2: Water | ChemComp-HOH / |
-Experimental details
-Experiment
Experiment | Method: X-RAY DIFFRACTION |
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-Sample preparation
Crystal | Density Matthews: 2.3 Å3/Da / Density % sol: 46.43 % | ||||||||||||||||||||||||||||||||||||||||
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Crystal grow | Temperature: 295 K / Method: vapor diffusion / pH: 6.8 / Details: pH 6.80, VAPOR DIFFUSION, temperature 295.00K | ||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Temperature: 295 K / pH: 6.8 / Method: vapor diffusion, sitting drop | ||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 295 K |
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Diffraction source | Source: ROTATING ANODE / Type: RIGAKU RU200 |
Detector | Type: RIGAKU AFC-5 / Detector: DIFFRACTOMETER |
Radiation | Scattering type: x-ray |
Radiation wavelength | Relative weight: 1 |
Reflection | Highest resolution: 2.5 Å / Num. all: 1861 / Num. obs: 1757 / Observed criterion σ(F): 1 |
Reflection | *PLUS Highest resolution: 2.5 Å / Observed criterion σ(F): 1 |
-Processing
Software | Name: NUCLSQ / Classification: refinement | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
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Refinement | Resolution: 2.5→6 Å / σ(F): 1 /
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Refine Biso |
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Refinement step | Cycle: LAST / Resolution: 2.5→6 Å
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Refine LS restraints |
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Refinement | *PLUS Highest resolution: 2.5 Å / Lowest resolution: 6 Å / σ(F): 1 | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Solvent computation | *PLUS | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Displacement parameters | *PLUS |