Text: THE STRUCTURES WERE DETERMINED FROM 2D NOESY EXPERIMENTS PERFORMED BOTH IN H2O AND D2O. THE DISTANCE RESTRAINTS DETERMINED FROM MARDIGRAS WERE BASED ON INTENSITIES FROM A NOESY WITH A MIXING ...Text: THE STRUCTURES WERE DETERMINED FROM 2D NOESY EXPERIMENTS PERFORMED BOTH IN H2O AND D2O. THE DISTANCE RESTRAINTS DETERMINED FROM MARDIGRAS WERE BASED ON INTENSITIES FROM A NOESY WITH A MIXING TIME OF 300MS. DQF-COSY AND H-P COSY WERE USED TO ASCERTAIN INFORMATION ABOUT THE TORSION ANGLES.
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試料調製
詳細
内容: WATER
試料状態
イオン強度: 30mM / pH: 7 / 圧: NORMAL / 温度: 303 K
結晶化
*PLUS
手法: other / 詳細: NMR
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NMR測定
NMRスペクトロメーター
タイプ: Bruker DRX500 / 製造業者: Bruker / モデル: DRX500 / 磁場強度: 500 MHz