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Structure paper

TitleNew insights into the oxidation process from neutron and X-ray crystal structures of an O 2 -sensitive [NiFe]-hydrogenase.
Journal, issue, pagesChem Sci, Vol. 14, Page 9306-9315, Year 2023
Publish dateAug 30, 2023 (structure data deposition date)
AuthorsHiromoto, T. / Nishikawa, K. / Inoue, S. / Ogata, H. / Hori, Y. / Kusaka, K. / Hirano, Y. / Kurihara, K. / Shigeta, Y. / Tamada, T. / Higuchi, Y.
External linksChem Sci / PubMed:37712026
MethodsX-ray diffraction / neutron diffraction
Resolution1.04 Å
Structure data

PDB-8w6x:
Neutron structure of [NiFe]-hydrogenase from D. vulgaris Miyazaki F in its oxidized state
Method: X-RAY DIFFRACTION / NEUTRON DIFFRACTION / Resolution: 1.04 Å

Chemicals

ChemComp-NFU:
formyl[bis(hydrocyanato-1kappaC)]ironnickel(Fe-Ni)

ChemComp-MPD:
(4S)-2-METHYL-2,4-PENTANEDIOL / precipitant*YM

ChemComp-OH:
HYDROXIDE ION

ChemComp-MG:
Unknown entry

ChemComp-CL:
Unknown entry

ChemComp-SF4:
IRON/SULFUR CLUSTER

ChemComp-F3S:
FE3-S4 CLUSTER

ChemComp-HOH:
WATER

Source
  • desulfovibrio vulgaris str. 'miyazaki f' (bacteria)
KeywordsOXIDOREDUCTASE / Hydrogenase / NiFe complex / FeS cluster / Oxidized state

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