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Structure paper

TitleInsights into the Desaturation of Cyclopeptin and its C3 Epimer Catalyzed by a non-Heme Iron Enzyme: Structural Characterization and Mechanism Elucidation.
Journal, issue, pagesAngew. Chem. Int. Ed. Engl., Vol. 57, Page 1831-1835, Year 2018
Publish dateAug 17, 2017 (structure data deposition date)
AuthorsLiao, H.J. / Li, J. / Huang, J.L. / Davidson, M. / Kurnikov, I. / Lin, T.S. / Lee, J.L. / Kurnikova, M. / Guo, Y. / Chan, N.L. / Chang, W.C.
External linksAngew. Chem. Int. Ed. Engl. / PubMed:29314482
MethodsX-ray diffraction
Resolution1.96 - 2.05 Å
Structure data

PDB-5y7r:
Quaternary complex of AsqJ-Fe3+-2OG-cyclopeptin
Method: X-RAY DIFFRACTION / Resolution: 1.96 Å

PDB-5y7t:
Quaternary complex of AsqJ-Fe3+-2OG-D-cyclopeptin
Method: X-RAY DIFFRACTION / Resolution: 2.05 Å

Chemicals

ChemComp-FE:
Unknown entry

ChemComp-AKG:
2-OXOGLUTARIC ACID

ChemComp-58K:
cyclopeptin

ChemComp-HOH:
WATER

ChemComp-8R0:
(3R)-4-methyl-3-(phenylmethyl)-1,3-dihydro-1,4-benzodiazepine-2,5-dione

Source
  • emericella nidulans (strain fgsc a4 / atcc 38163 / cbs 112.46 / nrrl 194 / m139) (mold)
KeywordsOXIDOREDUCTASE / Initial step for olefination / octahedron / ferric / initial step / D-cyclopeptin

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