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TitleSynthesis of Densely Phosphorylated Bis-1,5-Diphospho-myo-Inositol Tetrakisphosphate and its Enantiomer by Bidirectional P-Anhydride Formation.
Journal, issue, pagesAngew. Chem. Int. Ed. Engl., Vol. 53, Page 9508-9511, Year 2014
Publish dateApr 14, 2014 (structure data deposition date)
AuthorsCapolicchio, S. / Wang, H. / Thakor, D.T. / Shears, S.B. / Jessen, H.J.
External linksAngew. Chem. Int. Ed. Engl. / PubMed:25044992
MethodsX-ray diffraction
Resolution1.85 - 1.9 Å
Structure data

PDB-4q4c:
Crystal structure of the catalytic domain of human diphosphoinositol pentakisphosphate kinase 2 (PPIP5K2) in complex with ADP and synthetic 1,5-(PP)2-IP4 (1,5-IP8)
Method: X-RAY DIFFRACTION / Resolution: 1.9 Å

PDB-4q4d:
Crystal structure of the catalytic domain of human diphosphoinositol pentakisphosphate kinase 2 (PPIP5K2) in complex with AMP-PNP and synthetic 3,5-(PP)2-IP4 (3,5-IP8)
Method: X-RAY DIFFRACTION / Resolution: 1.85 Å

Chemicals

ChemComp-ADP:
ADENOSINE-5'-DIPHOSPHATE / ADP, energy-carrying molecule*YM

ChemComp-I8P:
(1R,3S,4R,5S,6R)-2,4,5,6-tetrakis(phosphonooxy)cyclohexane-1,3-diyl bis[trihydrogen (diphosphate)]

ChemComp-MG:
Unknown entry

ChemComp-HOH:
WATER

ChemComp-ANP:
PHOSPHOAMINOPHOSPHONIC ACID-ADENYLATE ESTER / AMP-PNP, energy-carrying molecule analogue*YM

ChemComp-2YN:
(1R,3S,4S,5R,6S)-2,4,5,6-tetrakis(phosphonooxy)cyclohexane-1,3-diyl bis[trihydrogen (diphosphate)]

Source
  • homo sapiens (human)
KeywordsTRANSFERASE / kinase / synthesis / inositol pyrophosphate / enantiomer

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