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Structure paper

TitleCrystal structure of a pre-acylation complex of the beta-lactamase inhibitor, sulbactam, bound to a sulfenamide bond containing thiol-beta-lactamase
Journal, issue, pagesJ. Am. Chem. Soc., Vol. 134, Page 16798-16804, Year 2012
Publish dateMay 26, 2012 (structure data deposition date)
AuthorsRodkey, E.A. / Drawz, S.M. / Sampson, J.M. / Bethel, C.R. / Bonomo, R.A. / van den Akker, F.
External linksJ. Am. Chem. Soc. / PubMed:22974281
MethodsX-ray diffraction
Resolution1.09 - 1.52 Å
Structure data

PDB-4fd8:
Structure of apo S70C SHV beta-lactamase
Method: X-RAY DIFFRACTION / Resolution: 1.52 Å

PDB-4fh2:
Structure of s70c beta-lactamase bound to sulbactam
Method: X-RAY DIFFRACTION / Resolution: 1.44 Å

PDB-4fh4:
high-resolution structure of apo wt SHV-1 beta-lactamase
Method: X-RAY DIFFRACTION / Resolution: 1.09 Å

Chemicals

ChemComp-MA4:
CYCLOHEXYL-HEXYL-BETA-D-MALTOSIDE

ChemComp-HOH:
WATER

ChemComp-0RN:
SULBACTAM / antibiotic, inhibitor*YM

Source
  • klebsiella pneumoniae (bacteria)
KeywordsHYDROLASE / class A beta-lactamase / hydrolase-hydrolase inhibitor complex / hydrolase/hydrolase inhibitor

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