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Structure paper

TitleX-ray and NMR Crystallography in an Enzyme Active Site: The Indoline Quinonoid Intermediate in Tryptophan Synthase.
Journal, issue, pagesJ. Am. Chem. Soc., Vol. 133, Page 4-7, Year 2011
Publish dateNov 29, 2010 (structure data deposition date)
AuthorsLai, J. / Niks, D. / Wang, Y. / Domratcheva, T. / Barends, T.R. / Schwarz, F. / Olsen, R.A. / Elliott, D.W. / Fatmi, M.Q. / Chang, C.E. ...Lai, J. / Niks, D. / Wang, Y. / Domratcheva, T. / Barends, T.R. / Schwarz, F. / Olsen, R.A. / Elliott, D.W. / Fatmi, M.Q. / Chang, C.E. / Schlichting, I. / Dunn, M.F. / Mueller, L.J.
External linksJ. Am. Chem. Soc. / PubMed:21142052
MethodsX-ray diffraction
Resolution1.85 Å
Structure data

PDB-3pr2:
Tryptophan synthase indoline quinonoid structure with F9 inhibitor in alpha site
Method: X-RAY DIFFRACTION / Resolution: 1.85 Å

Chemicals

ChemComp-F9F:
2-({[4-(TRIFLUOROMETHOXY)PHENYL]SULFONYL}AMINO)ETHYL DIHYDROGEN PHOSPHATE

ChemComp-7MN:
(Z)-N-[(1E)-1-carboxy-2-(2,3-dihydro-1H-indol-1-yl)ethylidene]{3-hydroxy-2-methyl-5-[(phosphonooxy)methyl]pyridin-4(1H)-ylidene}methanaminium

ChemComp-CS:
Unknown entry

ChemComp-HOH:
WATER

Source
  • salmonella enterica subsp. enterica serovar typhimurium (bacteria)
KeywordsLYASE / alpha-beta barrel / TIM-barrel / tryptophan synthesis

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