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Structure paper

TitleObserving enzyme ternary transition state analogue complexes by19F NMR spectroscopy.
Journal, issue, pagesChem Sci, Vol. 8, Page 8427-8434, Year 2017
Publish dateJul 28, 2017 (structure data deposition date)
AuthorsAmpaw, A. / Carroll, M. / von Velsen, J. / Bhattasali, D. / Cohen, A. / Bowler, M.W. / Jakeman, D.L.
External linksChem Sci / PubMed:29619190
MethodsX-ray diffraction
Resolution1.38 - 2.28 Å
Structure data

PDB-5olw:
5-fluorotryptophan labeled beta-phosphoglucomutase in an open conformation
Method: X-RAY DIFFRACTION / Resolution: 2.28 Å

PDB-5olx:
5-fluorotryptophan labeled beta-phosphoglucomutase in a closed conformation, orthorhomic crystal form
Method: X-RAY DIFFRACTION / Resolution: 1.38 Å

PDB-5oly:
5-fluorotryptophan labeled beta-phosphoglucomutase in a closed conformation, monoclinic crystal form
Method: X-RAY DIFFRACTION / Resolution: 2 Å

Chemicals

ChemComp-CA:
Unknown entry

ChemComp-HOH:
WATER

ChemComp-MG:
Unknown entry

ChemComp-BG6:
6-O-phosphono-beta-D-glucopyranose

ChemComp-MGF:
TRIFLUOROMAGNESATE

ChemComp-G6P:
6-O-phosphono-alpha-D-glucopyranose

Source
  • lactococcus lactis subsp. lactis (strain il1403) (lactic acid bacteria)
  • lactococcus lactis subsp. lactis (lactic acid bacteria)
KeywordsISOMERASE / phosphoryl transfer / NMR labeling / 19F-NMR

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