Mass: 18.015 Da / Num. of mol.: 32 / Source method: isolated from a natural source / Formula: H2O
-
Experimental details
-
Experiment
Experiment
Method: X-RAY DIFFRACTION / Number of used crystals: 1
-
Sample preparation
Crystal
Density % sol: 84.84 %
Crystal grow
Temperature: 277 K / Method: vapor diffusion, hanging drop Details: contained 2.8-3.4 M ammonium sulfate in 0.05-0.1 M NaAcO buffer, pH 5.2-5.6 PH range: 5.2-5.6
Resolution: 2.7→49.34 Å / Cor.coef. Fo:Fc: 0.927 / Cor.coef. Fo:Fc free: 0.939 / SU B: 12.971 / SU ML: 0.223 / Cross valid method: THROUGHOUT / ESU R: 0.242 / ESU R Free: 0.203 / Stereochemistry target values: MAXIMUM LIKELIHOOD / Details: HYDROGENS HAVE BEEN ADDED IN THE RIDING POSITIONS
Rfactor
Num. reflection
% reflection
Selection details
Rfree
0.25378
1725
5 %
RANDOM
Rwork
0.24496
-
-
-
obs
0.24541
32815
99.95 %
-
Solvent computation
Ion probe radii: 0.8 Å / Shrinkage radii: 0.8 Å / VDW probe radii: 1.2 Å / Solvent model: MASK