1: CIS PROLINE - PRO 168 2: THE O ATOM OF SER 221, WHICH IS CONTAINED IN THE ACTIVE SITES, WAS MODIFIED WITH PHENYLMETHYLSULFONYLFLUORIDE (PMSF); HOWEVER, THE PMSF GROUP WAS NOT CONSTRUCTED DUE TO THE LACK OF ELECTRON DENSITY.
THE O ATOM OF SER 221, WHICH IS CONTAINED IN THE ACTIVE SITES, WAS MODIFIED WITH ...THE O ATOM OF SER 221, WHICH IS CONTAINED IN THE ACTIVE SITES, WAS MODIFIED WITH PHENYLMETHYLSULFONYLFLUORIDE (PMSF); HOWEVER, THE PMSF GROUP WAS NOT CONSTRUCTED DUE TO THE LACK OF ELECTRON DENSITY.
配列の詳細
THE AMINO ACI SEQUENCE FOR THIS ENTRY IS FROM HAKAMADA, Y., KOBAYASHI, T., HITOMI, J., KAWAI, S. & ...THE AMINO ACI SEQUENCE FOR THIS ENTRY IS FROM HAKAMADA, Y., KOBAYASHI, T., HITOMI, J., KAWAI, S. & ITO, S. (1994) J. FERMET. BIOENG., ACCEPTED FOR PUBLICATION.
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実験情報
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実験
実験
手法: X線回折
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試料調製
結晶
マシュー密度: 2.22 Å3/Da / 溶媒含有率: 44.56 %
結晶化
*PLUS
温度: 291 K / pH: 5.5 / 手法: 蒸気拡散法, ハンギングドロップ法
溶液の組成
*PLUS
ID
濃度
一般名
Crystal-ID
Sol-ID
1
10mg/ml
enzyme
1
drop
2
50mM
acetate
1
drop
3
50mM
acetate
1
reservoir
4
1.4M
ammoniumsulphate
1
reservoir
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データ収集
放射
散乱光タイプ: x-ray
放射波長
相対比: 1
反射
*PLUS
最高解像度: 2.4 Å / 最低解像度: 100 Å / Num. obs: 7897 / % possible obs: 80.6 % / Num. measured all: 24185 / Rmerge(I) obs: 0.119