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Open data
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Basic information
Entry | Database: PDB / ID: 1f6i | ||||||||||||||||||
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Title | CRYSTAL STRUCTURE OF THE E-DNA HEXAMER GGCGM5CC | ||||||||||||||||||
![]() | DNA (5'-D(*![]() ![]() ![]() ![]() Function / homology | ![]() ![]() Method | ![]() ![]() ![]() Vargason, J.M. / Eichman, B.F. / Ho, P.S. | ![]() ![]() Title: The extended and eccentric E-DNA structure induced by cytosine methylation or bromination. Authors: Vargason, J.M. / Eichman, B.F. / Ho, P.S. History |
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Structure visualization
Structure viewer | Molecule: ![]() ![]() |
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Downloads & links
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Download
PDBx/mmCIF format | ![]() | 14.5 KB | Display | ![]() |
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PDB format | ![]() | 9.4 KB | Display | ![]() |
PDBx/mmJSON format | ![]() | Tree view | ![]() | |
Others | ![]() |
-Validation report
Arichive directory | ![]() ![]() | HTTPS FTP |
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-Related structure data
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Links
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Assembly
Deposited unit | ![]()
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1 |
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Unit cell |
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Components
#1: DNA chain | Mass: 1824.232 Da / Num. of mol.: 2 / Source method: obtained synthetically #2: Water | ChemComp-HOH / | ![]() |
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-Experimental details
-Experiment
Experiment | Method: ![]() |
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Sample preparation
Crystal | Density Matthews: 3.7 Å3/Da / Density % sol: 66.78 % | ||||||||||||||||||||||||||||||||||||||||||
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Crystal grow![]() | Temperature: 298 K / Method: vapor diffusion, sitting drop / pH: 6 Details: MGCL2, SPERMINE, SODIUM CACODYLATE, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K | ||||||||||||||||||||||||||||||||||||||||||
Components of the solutions |
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Crystal grow | *PLUS Method: vapor diffusion | ||||||||||||||||||||||||||||||||||||||||||
Components of the solutions | *PLUS
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-Data collection
Diffraction | Mean temperature: 298 K |
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Diffraction source | Source: ![]() |
Detector | Type: RIGAKU RAXIS IV / Detector: IMAGE PLATE / Date: Dec 2, 1999 |
Radiation | Protocol: SINGLE WAVELENGTH / Monochromatic (M) / Laue (L): M / Scattering type: x-ray |
Radiation wavelength | Wavelength![]() |
Reflection | Resolution: 2.2→500 Å / Num. all: 2571 / Num. obs: 2571 / % possible obs: 95.7 % / Observed criterion σ(F): 0 / Observed criterion σ(I): 0 / Redundancy: 9 % / Biso Wilson estimate: 36.2 Å2 / Rmerge(I) obs: 0.049 / Net I/σ(I): 28.1 |
Reflection shell | Resolution: 2.2→2.28 Å / Redundancy: 5 % / Rmerge(I) obs: 0.513 / % possible all: 91.6 |
Reflection | *PLUS Num. measured all: 23113 |
Reflection shell | *PLUS % possible obs: 91.6 % |
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Processing
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Refinement | Method to determine structure![]() ![]()
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Refinement step | Cycle: LAST / Resolution: 2.2→8 Å
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Refine LS restraints |
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