6Q8I
Nterminal domain of human SMU1 in complex with human REDmid
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 127.983, 68.163, 145.296 |
格子定数 [度] | 90.00, 109.40, 90.00 |
精密化法
残基 | 49.000 - 3.170 |
R因子 | 0.257 |
Rwork | 0.256 |
R-free | 0.27700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6q8f |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 0.980 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.2) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 49.000 | 3.250 |
分解能 [Å] (高) | 3.170 | 3.170 |
Rmeas | 0.144 | 1.146 |
独立反射数 | 39441 | 2828 |
<I/σ(I)> | 6.9 | 1.14 |
完全性 [%] | 94.3 | 97.2 |
冗長性 | 2.4 | 2.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Hepes pH 7.0-7.5, 8-10 % PEG 8K |