6P0S
Crystal structure of ternary DNA complex "FX2" containing E. coli Fis and phage lambda Xis
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97170 |
Spacegroup name | P 43 21 2 |
格子定数 [Å] | 107.670, 107.670, 150.430 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 87.550 - 2.700 |
R因子 | 0.222 |
Rwork | 0.222 |
R-free | 0.23000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6p0t |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.000 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (1.3.2) |
Refinement software | BUSTER (2.10.3) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 87.550 | 87.550 | 2.770 |
分解能 [Å] (高) | 2.700 | 12.090 | 2.700 |
Rmerge_l_obs | 0.116 | 0.123 | 0.492 |
Rmeas | 0.121 | 0.130 | 0.534 |
Total number of observations | 222119 | ||
独立反射数 | 23763 | 343 | 1528 |
<I/σ(I)> | 12.53 | 19.34 | 3.73 |
完全性 [%] | 95.6 | 100 | 85.1 |
冗長性 | 9.347 | 11.534 | 6.57 |
CC(1/2) | 0.998 | 0.998 | 0.915 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 15% PEG 4000 |