6OHT
Structure of EBP and U18666A
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 2 |
格子定数 [Å] | 194.566, 67.823, 96.858 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 48.642 - 3.200 |
R因子 | 0.2735 |
Rwork | 0.269 |
R-free | 0.31910 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.004 |
結合角の平均二乗偏差(RMSD) [度] | 0.927 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 3.260 |
分解能 [Å] (高) | 3.200 | 3.138 |
独立反射数 | 28389 | 2273 |
<I/σ(I)> | 30 | |
完全性 [%] | 99.8 | |
冗長性 | 12.9 | |
CC(1/2) | 0.990 | 0.739 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | Hepes, peg 600 |