6JYN
GII.13/21 noroviruses recognize glycans with a terminal beta-galactose via an unconventional glycan binding site
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 113 |
Detector technology | PIXEL |
Collection date | 2018-09-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97774 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 69.936, 122.935, 83.280 |
格子定数 [度] | 90.00, 90.07, 90.00 |
精密化法
残基 | 49.455 - 1.599 |
R因子 | 0.1864 |
Rwork | 0.181 |
R-free | 0.20070 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.660 |
分解能 [Å] (高) | 1.599 | 1.600 |
独立反射数 | 184076 | 184076 |
<I/σ(I)> | 18.333 | |
完全性 [%] | 99.5 | 97.5 |
冗長性 | 6.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M sodium citrate tribasic dehydrate, 20 percent polyethylene glycol 3350 |