6JP2

Crystal structure of pyrrolysyl-tRNA synthetase from Methanomethylophilus alvus

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.272 Å)

Cell axes112.380112.780107.430
Cell angles90.00114.2190.00
SpacegroupC 1 2 1
Resolution limits48.99 - 2.27
the highest resolution shell value2.311 - 2.272
R-factor0.2152
R-work0.21300
the highest resolution shell value0.285
R-free0.25670
the highest resolution shell value0.332
RMSD bond length0.002
RMSD bond angle0.513

Data Collection Statistics

Resolution limits49.00 - 2.27
the highest resolution shell value -
Number of reflections55681
Completeness99.0
Redundancy3.7
the highest resolution shell value3.5

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, SITTING DROP7.5293

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*