6JKW
Seleno-methionine PNGM-1 from deep-sea sediment metagenome
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-05-08 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97940 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 121.857, 83.124, 162.833 |
格子定数 [度] | 90.00, 110.18, 90.00 |
精密化法
残基 | 34.930 - 2.290 |
R因子 | 0.2143 |
Rwork | 0.211 |
R-free | 0.27420 |
Structure solution method | MAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.016 |
結合角の平均二乗偏差(RMSD) [度] | 1.725 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0029) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 34.930 | 2.340 |
分解能 [Å] (高) | 2.290 | 2.300 |
独立反射数 | 137843 | |
<I/σ(I)> | 4.7 | |
完全性 [%] | 98.1 | |
冗長性 | 3.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | EVAPORATION | 7 | 287 | 0.1M Tris-HCl, 0.2M MgCl2 and 10% PEG 8000 |