6IDV
Peptide Asparaginyl Ligases from Viola yedoensis
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.953723 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 156.800, 69.800, 104.480 |
格子定数 [度] | 90.00, 110.22, 90.00 |
精密化法
残基 | 48.000 - 2.400 |
R因子 | 0.219 |
Rwork | 0.195 |
R-free | 0.23630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5h0i |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.160 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | BUSTER (2.10.2) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.540 |
分解能 [Å] (高) | 2.400 | 2.400 |
Rmerge_l_obs | 0.210 | 1.240 |
独立反射数 | 41522 | 6542 |
<I/σ(I)> | 5.78 | |
完全性 [%] | 99.4 | |
冗長性 | 3.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | EVAPORATION | 293 | PEG 3350, 0.2m Magnesium formate |