Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-1A |
| Synchrotron site | Photon Factory |
| Beamline | BL-1A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-06-12 |
| Detector | DECTRIS EIGER R 4M |
| Wavelength(s) | 2.7 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 104.240, 156.830, 179.540 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.460 - 2.950 |
| R-factor | 0.1719 |
| Rwork | 0.170 |
| R-free | 0.20820 |
| Structure solution method | SAD |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXCD |
| Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.030 |
| High resolution limit [Å] | 2.950 | 2.950 |
| Number of reflections | 11135360 | 625357 |
| <I/σ(I)> | 52.23 | 3.29 |
| Completeness [%] | 99.9 | 99.5 |
| Redundancy | 177.76 | 137.02 |
| CC(1/2) | 1.000 | 0.823 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 6% PEG, 16% glycerol, 30 mM magnesium chloride, 30 mM calcium chloride, 0.1M MES/0.1M imidazole |
