6H8K
Crystal structure of a variant (Q133C in PSST) of Yarrowia lipolytica complex I
これはPDB形式変換不可エントリーです。
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0000 |
Spacegroup name | H 3 2 |
格子定数 [Å] | 316.310, 316.310, 819.180 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 40.000 - 3.790 |
R因子 | 0.361 |
Rwork | 0.361 |
R-free | 0.36300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wz7 |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.230 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.2) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 3.990 |
分解能 [Å] (高) | 3.790 | 3.790 |
Rmerge_l_obs | 0.204 | |
独立反射数 | 120019 | |
<I/σ(I)> | 13.2 | 0.7 |
完全性 [%] | 99.6 | |
冗長性 | 21 | |
CC(1/2) | 1.000 | 0.439 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 291 | PEG 3350, calcium acetate, glycerol |