6GF8
Molecular basis of egg coat filament cross-linking: structure of the glycosylated ZP1 ZP-N1 domain homodimer
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-07-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9791 |
Spacegroup name | C 2 2 21 |
格子定数 [Å] | 90.774, 125.734, 105.001 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 24.725 - 3.100 |
R因子 | 0.2127 |
Rwork | 0.210 |
R-free | 0.23520 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Monomer 6GF6 |
結合長の平均二乗偏差(RMSD) [Å] | 0.004 |
結合角の平均二乗偏差(RMSD) [度] | 0.657 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 42.740 | 3.240 |
分解能 [Å] (高) | 3.100 | 3.100 |
Rmeas | 0.093 | 1.114 |
Rpim | 0.043 | 0.520 |
独立反射数 | 11119 | 1328 |
<I/σ(I)> | 9.5 | 1 |
完全性 [%] | 99.1 | 96.9 |
冗長性 | 4.1 | 4.2 |
CC(1/2) | 1.000 | 0.650 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 29% (V/V) MPD, 0.1 M MES PH 6.5 |