6FMV
IMISX-EP of Hg-BacA soaking SIRAS
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-23 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.9 |
Spacegroup name | C 2 2 2 |
格子定数 [Å] | 113.390, 144.370, 40.390 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 40.390 - 2.300 |
R因子 | 0.1954 |
Rwork | 0.194 |
R-free | 0.22240 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXCD |
Refinement software | PHENIX ((1.12_2829: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 40.390 | 2.360 |
分解能 [Å] (高) | 2.300 | 2.300 |
Rmeas | 0.500 | 6.390 |
独立反射数 | 15224 | 2127 |
<I/σ(I)> | 9.85 | |
完全性 [%] | 100.0 | 100 |
冗長性 | 16.95 | 14.09 |
CC(1/2) | 0.990 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | LIPIDIC CUBIC PHASE | 293 | 40 % PEG-400, 0.3-0.5 M ammonium citrate dibasic and 0.1 M sodium citrate pH 5.0 |