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6EX9

Crystal Structure of HIV-1 Integrase Catalytic Core Domain with Inhibitor Peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-1
Synchrotron siteESRF
BeamlineID23-1
Temperature [K]100
Detector technologyCCD
Collection date2016-02-20
DetectorADSC QUANTUM 315r
Wavelength(s)0.97933
Spacegroup nameP 41 21 2
Unit cell lengths96.519, 96.519, 48.489
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution68.249 - 2.014
R-factor0.2284
Rwork0.226
R-free0.27930
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1bis
RMSD bond length0.007
RMSD bond angle0.841
Data reduction softwareMOSFLM
Data scaling softwareAimless
Phasing softwareREFMAC
Refinement softwarePHENIX ((1.11.1_2575: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]68.2602.086
High resolution limit [Å]2.0142.014
Rmerge0.0610.885
Rmeas0.067
Rpim0.029
Number of reflections156821524
<I/σ(I)>17.92.6
Completeness [%]100.099.93
Redundancy9.7
CC(1/2)0.996
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION2930.1 M Succinic acid, 15 % w/v PEG 3350

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건을2024-03-27부터공개중

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