6E4U
Structure of AMPK bound to activator
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-10-16 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 124.500, 124.500, 402.780 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 107.820 - 3.270 |
R-factor | 0.213 |
Rwork | 0.212 |
R-free | 0.23100 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.090 |
Data reduction software | autoXDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.7) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 107.820 | 3.390 |
High resolution limit [Å] | 3.270 | 3.270 |
Rmerge | 0.140 | 0.643 |
Number of reflections | 29561 | |
<I/σ(I)> | 19.7 | |
Completeness [%] | 100.0 | |
Redundancy | 16.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 750 MM AMMONIUM SULFATE, 500 MM LITHIUM SULFATE, 100 MM TRISODIUM CITRATE, 1% ETHYLENE GLYCOL |