6D2E

Crystal structure of Corynebacterium diphtheriae UDP-galactopyranose mutase in complex with UDP-galactopyranose (open, oxidized)

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (2.05 Å)

Cell axes98.41098.410127.820
Cell angles90.0090.0090.00
SpacegroupP 41 21 2
Resolution limits33.57 - 2.05
the highest resolution shell value2.123 - 2.050
R-factor0.1629
R-work0.16120
the highest resolution shell value0.230
R-free0.19560
the highest resolution shell value0.272
RMSD bond length0.008
RMSD bond angle1.091

Data Collection Statistics

Resolution limits33.57 - 2.05
the highest resolution shell value -
Number of reflections75195
Rmerge_l_obs0.101
the highest resolution shell value0.949
Completeness100.0
Redundancy29.3
the highest resolution shell value29.6

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
1VAPOR DIFFUSION, HANGING DROP8298

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*