6CUP
Ras:SOS:Ras in complex with a small molecule activator
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-F |
Synchrotron site | APS |
Beamline | 21-ID-F |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-01-31 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.98 |
Spacegroup name | I 4 2 2 |
格子定数 [Å] | 184.654, 184.654, 179.351 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 37.505 - 1.833 |
R因子 | 0.1608 |
Rwork | 0.161 |
R-free | 0.17380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4nyi |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 0.833 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13rc1_2961: ???)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.860 |
分解能 [Å] (高) | 1.830 | 1.830 |
Rpim | 0.039 | 0.414 |
独立反射数 | 134204 | |
<I/σ(I)> | 15.67 | |
完全性 [%] | 100.0 | |
冗長性 | 12 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293 | 0.1 M sodium acetate, 2.0 M sodium formate, pH 4.0 |