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5ZYI

Crystal structure of CERT START domain in complex with compound E16

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2017-07-22
DetectorRIGAKU RAXIS VII
Wavelength(s)1.5418
Spacegroup nameP 41 21 2
Unit cell lengths60.100, 60.100, 153.460
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.000 - 1.900
R-factor0.2158
Rwork0.214
R-free0.25280
RMSD bond length0.008
RMSD bond angle1.666
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0222)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]25.00025.0001.850
High resolution limit [Å]1.8008.0501.800
Rmerge0.0510.0190.957
Rmeas0.0550.0211.037
Number of reflections268723681968
<I/σ(I)>21.0155.81.81
Completeness [%]99.596.8100
Redundancy6.7985.4926.779
CC(1/2)0.9990.9990.693
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.92930.1M trisodium citrate/HCl buffer, pH 5.9, containing 24% PEG3350 and 0.2% n-octyl-beta-D-glucoside

217705

건을2024-03-27부터공개중

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