5ZQK
Dengue Virus Non Structural Protein 5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-07 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.980105 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 86.680, 146.100, 97.240 |
Unit cell angles | 90.00, 105.45, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.000 | 2.440 |
High resolution limit [Å] | 2.290 | 2.290 |
Number of reflections | 103117 | 16247 |
<I/σ(I)> | 8.62 | |
Completeness [%] | 99.7 | |
Redundancy | 3.89 | |
CC(1/2) | 0.996 | 0.631 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG 4000, Glycerol, Tris HCl, Bicine |