5YYN
Crystal structures of E.coli arginyl-trna synthetase (argrs) in complex with substrate TRNA(Arg)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-04-14 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.03988 |
Spacegroup name | P 65 |
格子定数 [Å] | 102.241, 102.241, 480.567 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 33.150 - 3.000 |
R因子 | 0.223 |
Rwork | 0.220 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bs2 |
結合長の平均二乗偏差(RMSD) [Å] | 0.003 |
結合角の平均二乗偏差(RMSD) [度] | 0.672 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 3.100 |
分解能 [Å] (高) | 3.000 | 3.000 |
Rmerge_l_obs | 0.456 | |
独立反射数 | 53802 | |
<I/σ(I)> | 13.2 | 2.9 |
完全性 [%] | 95.4 | 71.2 |
冗長性 | 10.5 | 7.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 5.6 | 290 | 0.1M NA3C6H5O7, 1.95M (NH4)2SO4, PH 5.6, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 290K |