5YC9
Crystal structure of a Pseudomonas aeruginosa transcriptional regulator
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-08 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.98 |
Spacegroup name | P 65 |
格子定数 [Å] | 111.642, 111.642, 261.137 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 34.323 - 2.900 |
R因子 | 0.2715 |
Rwork | 0.268 |
R-free | 0.30690 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_2875)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 35.000 | 2.950 |
分解能 [Å] (高) | 2.900 | 2.900 |
独立反射数 | 60294 | |
<I/σ(I)> | 18.71 | |
完全性 [%] | 100.0 | |
冗長性 | 7.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 10% v/v 1,4-Dioxane, 0.1 M MES pH 6.5, 1.6 M Ammonium sulfate |