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5XGQ

Crystal structure of apo form (free-state) Mycobacterium tuberculosis methionyl-tRNA synthetase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]100
Detector technologyAREA DETECTOR
Collection date2015-08-16
DetectorDECTRIS PILATUS 2M-F
Wavelength(s)1.000040
Spacegroup nameP 1
Unit cell lengths49.983, 72.727, 78.376
Unit cell angles98.90, 90.05, 98.47
Refinement procedure
Resolution48.686 - 1.899
R-factor0.2035
Rwork0.202
R-free0.23660
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2x1l
RMSD bond length0.003
RMSD bond angle0.589
Data reduction softwareXDS
Data scaling softwareXDS
Refinement softwarePHENIX ((1.10.1_2155: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.6862.010
High resolution limit [Å]1.8991.900
Rmerge0.0940.723
Number of reflections15872527608
<I/σ(I)>6.680.97
Completeness [%]93.1
Redundancy1.681.53
CC(1/2)0.9930.586
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1EVAPORATION6.12930.1M calcium acetate, 0.1M sodium cacodylate, 16%PEG8000

217705

數據於2024-03-27公開中

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