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5XF7

Crystal structure of human protein disulfide isomerase-like protein of the testis

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U1
Synchrotron siteSSRF
BeamlineBL17U1
Temperature [K]100
Detector technologyCCD
Collection date2015-11-11
DetectorAPEX II CCD
Wavelength(s)0.987
Spacegroup nameP 32
Unit cell lengths97.361, 97.361, 57.588
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution28.106 - 2.381
R-factor0.2003
Rwork0.197
R-free0.23520
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4ekz 4nwy
RMSD bond length0.008
RMSD bond angle0.957
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwarePHENIX ((1.10.1_2155: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.420
High resolution limit [Å]2.3802.380
Number of reflections24401
<I/σ(I)>20.62
Completeness [%]99.8100
Redundancy3.83.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP728921% (w/v) PEG 3350 and 0.1 M succinic acid, pH 7.0

217705

數據於2024-03-27公開中

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