5WXD

Crystal Structure of HLA-A*2402 in complex with avian influenza A(H7N9) virus-derived peptide H7-25 (data set 1)

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-04-15
Detector	SDMS
Wavelength(s)	1.03871
Spacegroup name	P 21 21 21
格子定数 [Å]	67.470, 78.983, 88.052
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	44.326 - 3.295
R因子	0.2052
Rwork	0.203
R-free	0.25400
結合長の平均二乗偏差(RMSD) [Å]	0.003
結合角の平均二乗偏差(RMSD) [度]	0.681
Data reduction software	CNS
Data scaling software	CNS
Phasing software	CNS
Refinement software	PHENIX ((1.10.1_2155))

Quality characteristics

	Overall
分解能 [Å] (低)	50.000
分解能 [Å] (高)	3.295
独立反射数	7564
<I/σ(I)>	12.175
完全性 [%]	86.4
冗長性	7.1

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	VAPOR DIFFUSION, HANGING DROP	7	291	0.1 M Imidazole pH 7.0, 12% w/v Polyethylene glycol 20000