5WWJ
Crystal Structure of HLA-A*2402 in complex with avian influenza A(H7N9) virus-derived peptide H7-25 (data set 1)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-28 |
Detector | SDMS |
Wavelength(s) | 0.97930 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 81.315, 67.272, 88.321 |
格子定数 [度] | 90.00, 98.41, 90.00 |
精密化法
残基 | 34.660 - 2.290 |
R因子 | 0.166 |
Rwork | 0.164 |
R-free | 0.21050 |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.222 |
Data reduction software | CNS |
Data scaling software | CNS |
Phasing software | CNS |
Refinement software | PHENIX ((1.10.1_2155)) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 50.000 |
分解能 [Å] (高) | 2.290 |
独立反射数 | 164558 |
<I/σ(I)> | 41.3 |
完全性 [%] | 99.1 |
冗長性 | 3.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 0.1 M Imidazole pH 7.0, 12% w/v Polyethylene glycol 20000 |