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5UFU

Structure of AMPK bound to activator

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2016-09-13
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)1
Spacegroup nameP 61 2 2
Unit cell lengths124.264, 124.264, 401.569
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution47.430 - 3.450
R-factor0.195
Rwork0.193
R-free0.23800
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.140
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareBUSTER (2.11.7)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]47.4303.510
High resolution limit [Å]3.4503.450
Rpim0.09535.400
Number of reflections25121
<I/σ(I)>9.9
Completeness [%]99.9
Redundancy8.1
CC(1/2)0.817
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293750 mM ammonium sulfate 500 mM lithium sulfate 100 mM trisodium citrate 1% ethylene glycol

217705

數據於2024-03-27公開中

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