5U2N
Crystal structure of human NAMPT with A-1326133
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 61.166, 107.049, 83.135 |
格子定数 [度] | 90.00, 96.77, 90.00 |
精密化法
残基 | 25.330 - 1.730 |
R因子 | 0.165 |
Rwork | 0.164 |
R-free | 0.19200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2gvj |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.040 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | BUSTER (2.11.7) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 107.000 |
分解能 [Å] (高) | 1.730 |
独立反射数 | 109253 |
<I/σ(I)> | 15 |
完全性 [%] | 97.9 |
冗長性 | 3.2 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 25% PEG 3350, 0.2 M ammonium sulfate, and 0.1 M HEPES, pH 7.5 |