5TDW
Set3 PHD finger in complex with histone H3K4me3
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-03-02 |
Detector | NOIR-1 |
Wavelength(s) | 1.00 |
Spacegroup name | P 2 21 21 |
格子定数 [Å] | 25.870, 43.680, 85.060 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 42.530 - 1.700 |
R因子 | 0.1662 |
Rwork | 0.165 |
R-free | 0.19910 |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.134 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 42.540 |
分解能 [Å] (高) | 1.700 |
独立反射数 | 11089 |
<I/σ(I)> | 14 |
完全性 [%] | 99.9 |
冗長性 | 26.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 273 | 20% PEG3350, 0.2 M sodium citrate |