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5PZY

Human liver fructose-1,6-bisphosphatase 1 (fructose 1,6-bisphosphate 1-phosphatase, E.C.3.1.3.11) complexed with the allosteric inhibitor 1-(5-bromo-1,3-thiazol-2-yl)-3-(2-chlorophenyl)sulfonylurea

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyCCD
Collection date2005-10-20
DetectorMAR CCD 165 mm
Wavelength(s)0.987
Spacegroup nameP 1 21 1
Unit cell lengths66.214, 283.778, 83.368
Unit cell angles90.00, 97.31, 90.00
Refinement procedure
Resolution24.255 - 2.210
R-factor0.1754
Rwork0.173
R-free0.22800
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle0.964
Refinement softwarePHENIX (1.11.1_2575)
Data quality characteristics
 Overall
Low resolution limit [Å]24.255
High resolution limit [Å]2.210
Number of reflections140872
Completeness [%]93.0
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP73000.1M HEPES pH 7.0, 0.1M AMMONIUM ACETATE, 12%-25% PEG 3350

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