5OE7
Structure of OTULIN bound to the Met1-linked diubiquitin activity probe
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 287 |
Detector technology | PIXEL |
Collection date | 2016-05-14 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | H 3 2 |
格子定数 [Å] | 101.143, 101.143, 277.916 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 54.430 - 2.950 |
R因子 | 0.227 |
Rwork | 0.223 |
R-free | 0.30900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3znz |
結合長の平均二乗偏差(RMSD) [Å] | 0.020 |
結合角の平均二乗偏差(RMSD) [度] | 2.157 |
Data scaling software | Aimless (0.5.27) |
Phasing software | PHASER (2.6.1) |
Refinement software | REFMAC (5.8.0158) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 54.430 | 3.130 |
分解能 [Å] (高) | 2.950 | 2.950 |
Rmerge_l_obs | 0.063 | 0.769 |
独立反射数 | 11908 | |
<I/σ(I)> | 13.6 | |
完全性 [%] | 100.0 | 100 |
冗長性 | 6.4 | 6.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 298 | 1.9-2.1 M Ammonium sulphate, 100 mM bis-tris |