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5MIM

Xray structure of human furin bound with the 2,5-dideoxystreptamine derived small molecule inhibitor 1n

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsBESSY BEAMLINE 14.1
Synchrotron siteBESSY
Beamline14.1
Temperature [K]100
Detector technologyPIXEL
Collection date2014-11-24
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.918409
Spacegroup nameP 65 2 2
Unit cell lengths132.204, 132.204, 155.727
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution41.694 - 1.900
R-factor0.1656
Rwork0.165
R-free0.18380
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5jxg
RMSD bond length0.007
RMSD bond angle1.070
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHENIX
Refinement softwarePHENIX (1.9_1692)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]46.1202.020
High resolution limit [Å]1.9001.900
Rmerge0.1310.791
Number of reflections63025
<I/σ(I)>11.042.17
Completeness [%]99.297.6
Redundancy4.94.8
CC(1/2)0.9960.732
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293.15CRYSTALLIZATION SOLUTION: 100 MM MES, 200 MM K/NAH2PO4, PH 5.5-6.0, 3-4 M NACL, 3% DMSO; RESERVOIR SOLUTION: 3-4 M NACL

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건을2024-03-27부터공개중

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