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5L6H

Uba1 in complex with Ub-ABPA3 covalent adduct

Replaces:  3CMMReplaces:  4NNJ
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE MASSIF-3
Synchrotron siteESRF
BeamlineMASSIF-3
Temperature [K]100
Detector technologyPIXEL
Collection date2016-02-28
DetectorDECTRIS EIGER X 4M
Wavelength(s)0.9686
Spacegroup nameP 2 21 21
Unit cell lengths72.048, 194.098, 230.172
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.300
R-factor0.17475
Rwork0.172
R-free0.21837
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4nnj
RMSD bond length0.023
RMSD bond angle2.216
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0135)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.000
High resolution limit [Å]2.3002.300
Number of reflections143279
<I/σ(I)>13.3
Completeness [%]99.5
Redundancy7.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP62930.2M lithium sulfate, 0.1M bis-tris, 15% peg 3350

217705

数据于2024-03-27公开中

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