5L3C
Human LSD1/CoREST: LSD1 E379K mutation
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-12-06 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 0.976256 |
Spacegroup name | I 2 2 2 |
格子定数 [Å] | 120.368, 180.389, 235.422 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 50.000 - 3.310 |
R因子 | 0.19906 |
Rwork | 0.199 |
R-free | 0.22324 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 2v1d |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.398 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0135) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 3.450 |
分解能 [Å] (高) | 3.300 | 3.300 |
Rmerge_l_obs | 0.130 | 0.800 |
独立反射数 | 38276 | |
<I/σ(I)> | 8.5 | 1.2 |
完全性 [%] | 99.0 | 99 |
冗長性 | 3.8 | 3.9 |
CC(1/2) | 0.990 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | Tartrate 1-1.4 M, ADA 100 mM pH 6.5 |